MX2016010692A - Proceso y sistema de produccion de acido acrilico. - Google Patents
Proceso y sistema de produccion de acido acrilico.Info
- Publication number
- MX2016010692A MX2016010692A MX2016010692A MX2016010692A MX2016010692A MX 2016010692 A MX2016010692 A MX 2016010692A MX 2016010692 A MX2016010692 A MX 2016010692A MX 2016010692 A MX2016010692 A MX 2016010692A MX 2016010692 A MX2016010692 A MX 2016010692A
- Authority
- MX
- Mexico
- Prior art keywords
- finishing column
- acrylic acid
- overhead
- stream
- aspirating
- Prior art date
Links
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 title 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 abstract 2
- 239000012808 vapor phase Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/50—Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/03—Monocarboxylic acids
- C07C57/04—Acrylic acid; Methacrylic acid
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un proceso de recuperación de ácido (met) acrílico incluye destilar una mezcla que comprende ácido (met) acrílico en una columna de acabado a menos de la presión atmosférica para producir una corriente de cabeza de la columna de acabado y una corriente de cola de la columna de acabado. Un sistema de condensador de contacto directo de aspiración de la cabeza condensa al menos parcialmente la corriente de cabeza de la columna de acabado para formar un condensado de cabeza de la columna de acabado y una corriente de ventilación de no condensables de la cabeza. También puede recuperarse una extracción lateral en fase vapor de la columna de acabado. Puede usarse un sistema de condensador de contacto directo de aspiración para condensar al menos parcialmente la extracción lateral en fase vapor.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201461942261P | 2014-02-20 | 2014-02-20 | |
| PCT/US2015/015520 WO2015126704A1 (en) | 2014-02-20 | 2015-02-12 | Process and system for producing acrylic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2016010692A true MX2016010692A (es) | 2017-05-09 |
Family
ID=53878832
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2016010692A MX2016010692A (es) | 2014-02-20 | 2015-02-12 | Proceso y sistema de produccion de acido acrilico. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US10112885B2 (es) |
| EP (1) | EP3110786B1 (es) |
| JP (1) | JP6703950B2 (es) |
| KR (1) | KR102327728B1 (es) |
| CN (1) | CN106061934B (es) |
| BR (1) | BR112016019248B1 (es) |
| MX (1) | MX2016010692A (es) |
| SA (1) | SA516371688B1 (es) |
| SG (1) | SG11201606743PA (es) |
| TW (1) | TWI658035B (es) |
| WO (1) | WO2015126704A1 (es) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3041958B1 (fr) * | 2015-10-06 | 2019-06-14 | Arkema France | Procede ameliore de production d’acide (meth)acrylique de grade polymere |
| DE202015106097U1 (de) * | 2015-11-11 | 2016-02-01 | Holger Blum | Fördereinrichtung für eine Vakuumdestillationsanlage |
| FR3049601B1 (fr) * | 2016-03-29 | 2018-03-09 | Arkema France | Procede ameliore de production d'acide (meth)acrylique |
| JP6522213B1 (ja) * | 2018-08-03 | 2019-05-29 | 住友化学株式会社 | メタクロレイン及び/又はメタクリル酸の製造方法 |
| FR3094716B1 (fr) | 2019-04-02 | 2021-06-04 | Arkema France | Production d’acide acrylique de grade polymere |
| FR3108906B1 (fr) | 2020-04-06 | 2022-03-04 | Arkema France | Procede de purification d’acide (meth)acrylique |
| KR102855131B1 (ko) * | 2021-10-15 | 2025-09-03 | 주식회사 엘지화학 | 아크릴산 제조방법 |
| KR102855127B1 (ko) * | 2021-10-15 | 2025-09-03 | 주식회사 엘지화학 | 아크릴산 제조방법 |
| CN114632343B (zh) * | 2022-05-18 | 2022-12-02 | 北京化工大学 | 一种mvr热泵精馏系统及方法 |
| KR102846320B1 (ko) * | 2022-09-14 | 2025-08-14 | 주식회사 엘지화학 | 아크릴산 제조방법 |
| KR20240037081A (ko) * | 2022-09-14 | 2024-03-21 | 주식회사 엘지화학 | 아크릴산 제조방법 |
| US20240093919A1 (en) * | 2022-09-19 | 2024-03-21 | Graham Corporation | Process vacuum system with condenser and dual ejectors |
| CN115738328B (zh) * | 2022-11-28 | 2024-07-19 | 东营市赫邦化工有限公司 | 一种节能的循环式甘油蒸馏蒸发器 |
| KR20240152019A (ko) * | 2023-04-12 | 2024-10-21 | 주식회사 엘지화학 | 젖산 탈수 반응을 통한 아크릴산 제조 방법 및 이의 제조 장치 |
| WO2025121919A1 (ko) * | 2023-12-07 | 2025-06-12 | 주식회사 엘지화학 | 아크릴산의 제조 방법 및 장치 |
| KR20250087112A (ko) * | 2023-12-07 | 2025-06-16 | 주식회사 엘지화학 | 아크릴산의 제조 방법 |
| FR3162750A1 (fr) * | 2024-05-30 | 2025-12-05 | Arkema France | Procede de purification d’acide (meth)acrylique |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3168136A (en) * | 1955-03-17 | 1965-02-02 | Babcock & Wilcox Co | Shell and tube-type heat exchanger |
| FR1357332A (fr) | 1962-05-18 | 1964-04-03 | Shell Int Research | Procédé d'amélioration de la résistance au choc des pièces moulées en polypropylène |
| US3301871A (en) | 1964-06-15 | 1967-01-31 | Upjohn Co | Novel 1, 4-dialkylprolines, derivatives thereof and process |
| US3314220A (en) * | 1965-03-22 | 1967-04-18 | Foster Wheeler Corp | Multiannular centrifugal separator |
| DE69320386T2 (de) * | 1992-02-28 | 1999-02-04 | Sumitomo Chemical Co., Ltd., Tokio/Tokio | Verfahren zur Herstellung von Isobutylen durch oxidative Dehydrierung von Isobutan |
| JP3411280B2 (ja) * | 1992-09-21 | 2003-05-26 | 協和醗酵工業株式会社 | 血小板減少症治療剤 |
| JPH10204030A (ja) * | 1997-01-24 | 1998-08-04 | Toagosei Co Ltd | (メタ)アクリル酸エステルの精製方法及び製造方法並びにその製造装置 |
| US6019820A (en) | 1997-05-07 | 2000-02-01 | E. I. Du Pont De Nemours And Company | Liquid jet compressor |
| DE19740253A1 (de) | 1997-09-12 | 1999-03-18 | Basf Ag | Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten |
| DE19837519A1 (de) * | 1998-08-19 | 2000-02-24 | Basf Ag | Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan |
| JP4698778B2 (ja) | 1999-06-03 | 2011-06-08 | 株式会社日本触媒 | (メタ)アクリル酸(エステル)の精製方法 |
| JP3948855B2 (ja) * | 1999-06-10 | 2007-07-25 | 株式会社日本触媒 | (メタ)アクリル酸の製造方法 |
| JP2001131116A (ja) | 1999-11-08 | 2001-05-15 | Nippon Shokubai Co Ltd | 易重合性物質含有液の蒸留方法 |
| CN1307145C (zh) | 2001-08-22 | 2007-03-28 | 三菱化学株式会社 | 容易聚合化合物用蒸馏装置 |
| JP2005179352A (ja) * | 2003-11-28 | 2005-07-07 | Mitsubishi Chemicals Corp | (メタ)アクリル酸の精製方法 |
| WO2008033687A2 (en) * | 2006-09-15 | 2008-03-20 | Dow Global Technologies Inc. | Process for producing acrylic acid |
| WO2009123872A1 (en) | 2008-04-01 | 2009-10-08 | Dow Global Technologies Inc. | Procedure for the startup of a (meth)acrylic acid plant |
| WO2010027732A1 (en) * | 2008-09-04 | 2010-03-11 | Dow Global Technologies Inc. | Process for producing acrolein and/or acrylic acid from propane |
| FR2935971B1 (fr) | 2008-09-16 | 2010-11-19 | Arkema France | Acide bio-acrylique de grade polymere et son procede de fabrication a partir de glycerol. |
| KR101994630B1 (ko) | 2008-10-01 | 2019-07-02 | 알케마 인코포레이티드 | 온라인 근적외선 분석을 이용한 (메트)아크릴산 정제 방법의 제어 |
| EP2179981A1 (en) | 2008-10-24 | 2010-04-28 | Arkema France | Process for manufacturing acrolein from glycerol |
-
2015
- 2015-02-12 JP JP2016553438A patent/JP6703950B2/ja active Active
- 2015-02-12 EP EP15751390.4A patent/EP3110786B1/en active Active
- 2015-02-12 KR KR1020167023211A patent/KR102327728B1/ko active Active
- 2015-02-12 BR BR112016019248-6A patent/BR112016019248B1/pt active IP Right Grant
- 2015-02-12 SG SG11201606743PA patent/SG11201606743PA/en unknown
- 2015-02-12 CN CN201580009720.7A patent/CN106061934B/zh active Active
- 2015-02-12 US US15/118,126 patent/US10112885B2/en active Active
- 2015-02-12 MX MX2016010692A patent/MX2016010692A/es unknown
- 2015-02-12 WO PCT/US2015/015520 patent/WO2015126704A1/en not_active Ceased
- 2015-02-17 TW TW104105708A patent/TWI658035B/zh not_active IP Right Cessation
-
2016
- 2016-08-18 SA SA516371688A patent/SA516371688B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CN106061934A (zh) | 2016-10-26 |
| US20170174604A1 (en) | 2017-06-22 |
| KR20160122749A (ko) | 2016-10-24 |
| TWI658035B (zh) | 2019-05-01 |
| EP3110786A4 (en) | 2017-09-06 |
| EP3110786B1 (en) | 2021-08-25 |
| SG11201606743PA (en) | 2016-09-29 |
| JP6703950B2 (ja) | 2020-06-03 |
| CN106061934B (zh) | 2019-05-03 |
| TW201534581A (zh) | 2015-09-16 |
| BR112016019248A2 (es) | 2017-08-15 |
| KR102327728B1 (ko) | 2021-11-18 |
| US10112885B2 (en) | 2018-10-30 |
| BR112016019248B1 (pt) | 2022-03-15 |
| JP2017509613A (ja) | 2017-04-06 |
| WO2015126704A1 (en) | 2015-08-27 |
| SA516371688B1 (ar) | 2019-04-16 |
| EP3110786A1 (en) | 2017-01-04 |
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