MX2015017254A - Un metodo para producir 2,3-dicloro-5-(triclorometil)piridina. - Google Patents
Un metodo para producir 2,3-dicloro-5-(triclorometil)piridina.Info
- Publication number
- MX2015017254A MX2015017254A MX2015017254A MX2015017254A MX2015017254A MX 2015017254 A MX2015017254 A MX 2015017254A MX 2015017254 A MX2015017254 A MX 2015017254A MX 2015017254 A MX2015017254 A MX 2015017254A MX 2015017254 A MX2015017254 A MX 2015017254A
- Authority
- MX
- Mexico
- Prior art keywords
- pyridine
- triclorometil
- dicloro
- produce
- pcl5
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 title 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 title 1
- XVBWGQSXLITICX-UHFFFAOYSA-N 2,3-dichloro-5-(trichloromethyl)pyridine Chemical compound ClC1=CC(C(Cl)(Cl)Cl)=CN=C1Cl XVBWGQSXLITICX-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000005660 chlorination reaction Methods 0.000 abstract 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/61—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/62—Oxygen or sulfur atoms
- C07D213/63—One oxygen atom
- C07D213/64—One oxygen atom attached in position 2 or 6
- C07D213/643—2-Phenoxypyridines; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invención se refiere a un nuevo proceso para producir 2,3-dicloro-5-(triclorometil) piridina utilizando PCl5 como agente de cloración a temperatura y presión elevadas.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DKPA201370319 | 2013-06-14 | ||
| DKPA201470138 | 2014-03-20 | ||
| PCT/DK2014/050166 WO2014198278A1 (en) | 2013-06-14 | 2014-06-13 | A method for producing 2,3-dichloro-5-(trichloromethyl)pyridine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2015017254A true MX2015017254A (es) | 2016-12-14 |
| MX384518B MX384518B (es) | 2025-03-14 |
Family
ID=50980092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2015017254A MX384518B (es) | 2013-06-14 | 2014-06-13 | Un metodo para producir 2,3-dicloro-5-(triclorometil)piridina. |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US9809543B2 (es) |
| EP (1) | EP3008040B1 (es) |
| JP (1) | JP6337102B2 (es) |
| KR (1) | KR102246104B1 (es) |
| CN (1) | CN105492425B (es) |
| BR (1) | BR112015031324B1 (es) |
| DK (1) | DK3008040T3 (es) |
| ES (1) | ES2632454T3 (es) |
| IL (1) | IL243083B (es) |
| MX (1) | MX384518B (es) |
| TW (1) | TWI629262B (es) |
| WO (1) | WO2014198278A1 (es) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104610137A (zh) * | 2015-01-30 | 2015-05-13 | 大连世慕化学有限公司 | 2-氯-5-三氯甲基吡啶及2-氯-5-三氟甲基吡啶合成方法 |
| CN106397309A (zh) * | 2016-08-31 | 2017-02-15 | 南京红太阳生物化学有限责任公司 | 一种2,3‑二氯‑5‑三氟甲基吡啶的合成方法 |
| WO2018186460A1 (ja) * | 2017-04-04 | 2018-10-11 | 石原産業株式会社 | トリフルオロメチルピリジン類の精製方法 |
| CN107473973A (zh) * | 2017-07-31 | 2017-12-15 | 山东福尔有限公司 | 一种6‑氯‑2‑硝基甲苯制备方法 |
| CN107814759A (zh) * | 2017-11-24 | 2018-03-20 | 常州沃腾化工科技有限公司 | 氟吡菌胺的制备方法 |
| EP3620451B1 (en) * | 2017-12-06 | 2022-09-21 | Zhejiang Lantian Environmental Protection Hi-Tech Co., Ltd. | Method for preparing 2,3-dichloro-5-trifluoromethylpyridine with high selectivity |
| CN108997203B (zh) * | 2018-06-26 | 2020-08-14 | 江苏扬农化工集团有限公司 | 一种2,3-二氯-5-三氟甲基吡啶的高效提纯方法 |
| CN109020879A (zh) * | 2018-09-30 | 2018-12-18 | 浙江海正化工股份有限公司 | 一种2-氯-3-三氯甲基吡啶的制备方法 |
| CN110038587B (zh) * | 2019-05-14 | 2022-08-12 | 中触媒新材料股份有限公司 | 一种用于合成2,3-二氯-5-三氟甲基吡啶的催化剂及其制备方法 |
| WO2021072774A1 (zh) * | 2019-10-18 | 2021-04-22 | 鲁南贝特制药有限公司 | 一种七氟醚的合成方法 |
| CN115160102B (zh) * | 2022-08-13 | 2024-02-06 | 上海珂华生物科技有限公司 | 一种偕二卤代物的制备方法 |
| CN115181060B (zh) * | 2022-08-19 | 2024-03-19 | 江苏禾裕泰化学有限公司 | 一种生产2-氨基-3-氯-5-三氟甲基吡啶的清洁生产工艺 |
| CN115322145A (zh) * | 2022-10-17 | 2022-11-11 | 潍坊新绿化工有限公司 | 一种高效氟吡甲禾灵的生产方法 |
| CN117964490B (zh) * | 2024-01-24 | 2024-12-20 | 景德镇富祥生命科技有限公司 | 一种三氟甲基芳香化合物的制备方法 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0001473B1 (en) | 1977-08-12 | 1988-07-27 | Imperial Chemical Industries Plc | Herbicidal halogenomethyl--pyridyloxy-phenoxy-alkanecarboxylic acids and derivatives, and processes of controlling unwanted plants therewith |
| GB2002368A (en) | 1977-08-12 | 1979-02-21 | Ici Ltd | Herbicidal 2-(4-Alkoxyphenyloxy) pyridine compounds |
| DE2967486D1 (en) | 1978-03-01 | 1985-08-29 | Ici Plc | Mixtures of herbicidal pyridyloxyphenoxypropanoic acid derivatives with other herbicides, and processes of killing unwanted plants therewith |
| JPS5543017A (en) | 1978-09-22 | 1980-03-26 | Ishihara Sangyo Kaisha Ltd | Preparation of 2-chloro-5-trichloromethylpyridine |
| IL63511A (en) * | 1980-08-21 | 1986-02-28 | Dow Chemical Co | Method for converting carboxylic acid groups to trichloromethyl groups |
| US4419514A (en) * | 1980-08-21 | 1983-12-06 | The Dow Chemical Company | Method for converting carboxylic acid groups to trichloromethyl groups |
| US4309548A (en) | 1981-01-19 | 1982-01-05 | The Dow Chemical Company | Chlorination of 2-chloro-5-trichloromethylpyridine |
| US4331811A (en) | 1981-03-12 | 1982-05-25 | The Dow Chemical Company | Preparation of 2,3-dichloro-5-trichloromethylpyridine |
| US4636565A (en) | 1981-03-12 | 1987-01-13 | The Dow Chemical Company | Preparation of 2,3-dichloro-5-trichloromethylpyridine |
| US4567273A (en) * | 1982-04-16 | 1986-01-28 | The Dow Chemical Company | Liquid phase halogen exchange of (trichloromethyl) pyridines to (trifluoromethyl)pyridines |
| IL70307A (en) * | 1982-11-26 | 1987-02-27 | Dow Chemical Co | Preparation of(trifluoromethyl)pyridines |
| US4701532A (en) * | 1983-03-25 | 1987-10-20 | The Dow Chemical Company | Method of selectively chlorinating 2-chloro-5-(trichloromethyl) pyridine in the 3-position |
| US4634771A (en) * | 1985-07-25 | 1987-01-06 | Stauffer Chemical Company | Method for converting carboxylic acid groups to trichloromethyl groups |
| US4672125A (en) * | 1985-12-13 | 1987-06-09 | The Dow Chemical Company | Chlorination of β-methylpyridine compounds |
| JPH0699394B2 (ja) * | 1986-05-31 | 1994-12-07 | ザ ダウ ケミカル カンパニ− | 2−クロロ−5−(トリクロロメチル)ピリジンの3−位置を選択的に塩素化する方法 |
| US4833250A (en) | 1986-06-30 | 1989-05-23 | Ici Americas Inc. | Process of converting a carboxylic acid or carboxylic acid halide group to a trihalomethyl group |
| EP0281965A1 (en) | 1987-03-09 | 1988-09-14 | Ici Americas Inc. | Method of converting a carboxylic acid or carboxylic acid halide group to a trihalomethyl group |
| DE3800179A1 (de) | 1988-01-07 | 1989-07-20 | Bayer Ag | Verfahren zur herstellung von 2-chlor-5-methyl-pyridin |
| DE58908969D1 (de) * | 1988-12-16 | 1995-03-16 | Bayer Ag | Verfahren zur Herstellung von 2-Chlor-5-chlormethylpyridin. |
| DE58908915D1 (de) | 1988-12-16 | 1995-03-02 | Bayer Ag | Verfahren zur Herstellung von 2-Chlor-5-chlormethylpyridin. |
| US5229519A (en) | 1992-03-06 | 1993-07-20 | Reilly Industries, Inc. | Process for preparing 2-halo-5-halomethylpyridines |
| US5484929A (en) | 1993-09-21 | 1996-01-16 | Reilly Industries | Chlorination process |
| CA2150540A1 (en) | 1992-12-15 | 1994-06-23 | Joseph E. Toomey | Chlorination process |
| DE60125378T2 (de) | 2000-08-25 | 2007-04-26 | Bayer Cropscience S.A. | Verfahren zur Herstellung von 2-AMINOMETHYL-HALOGEN-PYRIDINEN |
| WO2007060662A2 (en) * | 2005-11-23 | 2007-05-31 | Makhteshim Chemical Works Ltd. | Process for preparing pyridinamines and novel polymorphs thereof |
| CN100564359C (zh) | 2007-06-27 | 2009-12-02 | 上海康鹏化学有限公司 | 一种2,3-二氯-5-三氯甲基吡啶的制备方法 |
| CN101265228A (zh) * | 2008-04-30 | 2008-09-17 | 上海立科药物化学有限公司 | 2-氯-3-三氯甲基-6-三氟甲基吡啶的制备方法 |
-
2014
- 2014-06-13 JP JP2016518843A patent/JP6337102B2/ja active Active
- 2014-06-13 TW TW103120402A patent/TWI629262B/zh active
- 2014-06-13 US US14/898,416 patent/US9809543B2/en active Active
- 2014-06-13 EP EP14731903.2A patent/EP3008040B1/en active Active
- 2014-06-13 CN CN201480039988.0A patent/CN105492425B/zh active Active
- 2014-06-13 DK DK14731903.2T patent/DK3008040T3/en active
- 2014-06-13 MX MX2015017254A patent/MX384518B/es unknown
- 2014-06-13 KR KR1020167000954A patent/KR102246104B1/ko active Active
- 2014-06-13 BR BR112015031324-8A patent/BR112015031324B1/pt active IP Right Grant
- 2014-06-13 ES ES14731903.2T patent/ES2632454T3/es active Active
- 2014-06-13 WO PCT/DK2014/050166 patent/WO2014198278A1/en not_active Ceased
-
2015
- 2015-12-13 IL IL243083A patent/IL243083B/en active IP Right Grant
-
2017
- 2017-11-03 US US15/802,662 patent/US10442765B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| KR102246104B1 (ko) | 2021-04-29 |
| CN105492425A (zh) | 2016-04-13 |
| CN105492425B (zh) | 2018-03-27 |
| IL243083B (en) | 2018-10-31 |
| US10442765B2 (en) | 2019-10-15 |
| US20160145211A1 (en) | 2016-05-26 |
| TW201446739A (zh) | 2014-12-16 |
| BR112015031324A2 (pt) | 2017-07-25 |
| TWI629262B (zh) | 2018-07-11 |
| EP3008040A1 (en) | 2016-04-20 |
| KR20160042869A (ko) | 2016-04-20 |
| ES2632454T3 (es) | 2017-09-13 |
| MX384518B (es) | 2025-03-14 |
| US9809543B2 (en) | 2017-11-07 |
| EP3008040B1 (en) | 2017-04-05 |
| DK3008040T3 (en) | 2017-07-31 |
| BR112015031324B1 (pt) | 2020-05-12 |
| JP2016521730A (ja) | 2016-07-25 |
| US20180057459A1 (en) | 2018-03-01 |
| WO2014198278A1 (en) | 2014-12-18 |
| JP6337102B2 (ja) | 2018-06-06 |
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