MX2015012584A - ELECTROLYTIC GENERATION OF IONS OF MANGANESI (III) IN VERY IONIZED SULFURIC ACID. - Google Patents
ELECTROLYTIC GENERATION OF IONS OF MANGANESI (III) IN VERY IONIZED SULFURIC ACID.Info
- Publication number
- MX2015012584A MX2015012584A MX2015012584A MX2015012584A MX2015012584A MX 2015012584 A MX2015012584 A MX 2015012584A MX 2015012584 A MX2015012584 A MX 2015012584A MX 2015012584 A MX2015012584 A MX 2015012584A MX 2015012584 A MX2015012584 A MX 2015012584A
- Authority
- MX
- Mexico
- Prior art keywords
- ions
- iii
- plastic
- manganese
- electrolytic cell
- Prior art date
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title 2
- 239000008151 electrolyte solution Substances 0.000 abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 229910021397 glassy carbon Inorganic materials 0.000 abstract 2
- 239000002650 laminated plastic Substances 0.000 abstract 2
- -1 manganese (II) ions Chemical class 0.000 abstract 2
- 229910001437 manganese ion Inorganic materials 0.000 abstract 2
- 229920000049 Carbon (fiber) Polymers 0.000 abstract 1
- 229910000978 Pb alloy Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000010405 anode material Substances 0.000 abstract 1
- 239000004917 carbon fiber Substances 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 abstract 1
- 238000006056 electrooxidation reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/21—Manganese oxides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/2006—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30
- C23C18/2046—Pretreatment of the material to be coated of organic surfaces, e.g. resins by other methods than those of C23C18/22 - C23C18/30 by chemical pretreatment
- C23C18/2073—Multistep pretreatment
- C23C18/2086—Multistep pretreatment with use of organic or inorganic compounds other than metals, first
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/20—Pretreatment of the material to be coated of organic surfaces, e.g. resins
- C23C18/22—Roughening, e.g. by etching
- C23C18/24—Roughening, e.g. by etching using acid aqueous solutions
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/042—Electrodes formed of a single material
- C25B11/043—Carbon, e.g. diamond or graphene
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
- C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
- C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
- C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
- C25B11/075—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound
- C25B11/081—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound the element being a noble metal
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/02—Process control or regulation
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
- C25D5/54—Electroplating of non-metallic surfaces
- C25D5/56—Electroplating of non-metallic surfaces of plastics
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Automation & Control Theory (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Chemically Coating (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
Se describe una celda electrolítica y un método de oxidación electroquímica de los iones de manganeso (II) a iones de manganeso (III) en la celda electrolítica. La celda electrolítica comprende (1) una solución electrolítica de iones manganeso (II) en una solución de al menos un ácido; (2) un cátodo sumergido en la solución electrolítica; y (3) un ánodo sumergido en la solución electrolítica y separado del cátodo. Diversos materiales de ánodo se describen incluyendo carbono vítreo, carbono vítreo reticulado, fibras de carbono tejidas, plomo y aleaciones de plomo. Una vez que el electrolito se oxida para formar un complejo metaestable de iones manganeso (III), un plástico laminable puede ponerse en contacto con el complejo metaestable para el ataque químico del plástico laminable. Además, una etapa de pretratamiento puede realizarse también en el plástico laminable antes de poner en contacto el plástico laminable con el complejo metaestable para acondicionar la superficie de plástico.An electrolytic cell and an electrochemical oxidation method of manganese (II) ions to manganese (III) ions in the electrolytic cell are described. The electrolytic cell comprises (1) an electrolytic solution of manganese ions (II) in a solution of at least one acid; (2) a cathode immersed in the electrolyte solution; and (3) an anode immersed in the electrolyte solution and separated from the cathode. Various anode materials are described including vitreous carbon, crosslinked vitreous carbon, woven carbon fibers, lead and lead alloys. Once the electrolyte oxidizes to form a metastable complex of manganese ions (III), a laminated plastic can contact the metastable complex for chemical attack of the laminable plastic. In addition, a pretreatment step can also be carried out in the laminated plastic before contacting the laminable plastic with the metastable complex to condition the plastic surface.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/795,382 US9534306B2 (en) | 2012-01-23 | 2013-03-12 | Electrolytic generation of manganese (III) ions in strong sulfuric acid |
| PCT/US2014/021618 WO2014164272A1 (en) | 2013-03-12 | 2014-03-07 | Electrolytic generation of manganese (iii) ions in strong sulfuric acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2015012584A true MX2015012584A (en) | 2016-01-14 |
| MX379432B MX379432B (en) | 2025-03-10 |
Family
ID=51658840
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2015012584A MX379432B (en) | 2013-03-12 | 2014-03-07 | Electrolytic generation of manganese (iii) ions in strong sulfuric acid |
Country Status (18)
| Country | Link |
|---|---|
| EP (1) | EP2971260B1 (en) |
| JP (1) | JP6167222B2 (en) |
| KR (1) | KR101749947B1 (en) |
| CN (1) | CN105209667B (en) |
| AU (1) | AU2014249521B2 (en) |
| BR (1) | BR112015021067B1 (en) |
| CA (2) | CA2901589C (en) |
| DK (1) | DK2971260T3 (en) |
| ES (1) | ES2745071T3 (en) |
| HR (1) | HRP20191626T1 (en) |
| HU (1) | HUE045344T2 (en) |
| LT (1) | LT2971260T (en) |
| MX (1) | MX379432B (en) |
| PL (1) | PL2971260T3 (en) |
| PT (1) | PT2971260T (en) |
| SI (1) | SI2971260T1 (en) |
| TW (1) | TWI489007B (en) |
| WO (1) | WO2014164272A1 (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9267077B2 (en) * | 2013-04-16 | 2016-02-23 | Rohm And Haas Electronic Materials Llc | Chrome-free methods of etching organic polymers with mixed acid solutions |
| MX368631B (en) * | 2013-10-22 | 2019-10-08 | Okuno Chem Ind Co | Composition for etching treatment of resin material. |
| CN105483715B (en) * | 2015-12-09 | 2018-01-30 | 哈尔滨工业大学 | The template 3D etching preparation methods of the micro-nano combined multi-stage Porous materials of magnesium based metal |
| CN106830204B (en) * | 2017-03-13 | 2020-04-28 | 重庆大学 | Method and device for degrading pollutants in water by exciting permanganate through electrochemical cathode |
| EP3652360A1 (en) * | 2017-07-10 | 2020-05-20 | SRG Global, Inc. | Hexavalent chromium free etch manganese recovery system |
| CN109256180B (en) * | 2018-07-03 | 2022-02-11 | 南昌立德生物技术有限公司 | Sensitivity analysis algorithm for computer-aided pilot medicament optimization design |
| JP7336126B2 (en) * | 2019-03-11 | 2023-08-31 | 国立研究開発法人産業技術総合研究所 | High-value manganese production method and production apparatus |
| EP3825441A1 (en) * | 2019-11-21 | 2021-05-26 | COVENTYA S.p.A. | An electrolytic treatment device for preparing plastic parts to be metallized and a method for etching plastic parts |
| US11842958B2 (en) * | 2022-03-18 | 2023-12-12 | Chun-Ming Lin | Conductive structure including copper-phosphorous alloy and a method of manufacturing conductive structure |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3065155A (en) | 1960-09-02 | 1962-11-20 | Manganese Chemicals Corp | Electrolytic manganese dioxide process |
| US3793171A (en) * | 1970-09-04 | 1974-02-19 | Carrier Corp | Process for removing pollutants from gas streams |
| JPS51764A (en) * | 1974-06-25 | 1976-01-06 | Mitsui Mining & Smelting Co | MUDENKAIDOMETSUKIHAISUINO SHORIHOHO |
| US3941677A (en) * | 1974-06-27 | 1976-03-02 | Carrier Corporation | Electrolytic regeneration cell |
| AU4083878A (en) * | 1977-11-02 | 1980-04-24 | Diamond Shamrock Techn | Dislodging electrolytic manganese dioxide |
| US4279705A (en) * | 1980-02-19 | 1981-07-21 | Kerr-Mcgee Corporation | Process for oxidizing a metal of variable valence by constant current electrolysis |
| JPS6013087A (en) * | 1983-07-05 | 1985-01-23 | Kawasaki Kasei Chem Ltd | Electrolysis method of cerous sulfate |
| JPS6447890A (en) * | 1987-08-13 | 1989-02-22 | Kenzo Yamaguchi | Electrolytic synthesis method |
| US5213665A (en) * | 1988-02-29 | 1993-05-25 | Nippon Shokubai Kagaku Kogyo, Co., Ltd. | Process for producing 1-aminoanthraquinones |
| US4911802A (en) * | 1988-03-09 | 1990-03-27 | Macdermid, Incorporated | Conversion of manganate to permanganate |
| US4936970A (en) * | 1988-11-14 | 1990-06-26 | Ebonex Technologies, Inc. | Redox reactions in an electrochemical cell including an electrode comprising Magneli phase titanium oxide |
| US5318803A (en) * | 1990-11-13 | 1994-06-07 | International Business Machines Corporation | Conditioning of a substrate for electroless plating thereon |
| JPH05112872A (en) * | 1991-10-21 | 1993-05-07 | Okuno Seiyaku Kogyo Kk | Method for electroless-plating polyimide resin and pre-etching composition |
| US5246553A (en) * | 1992-03-05 | 1993-09-21 | Hydro-Quebec | Tetravalent titanium electrolyte and trivalent titanium reducing agent obtained thereby |
| JP3806181B2 (en) * | 1996-05-31 | 2006-08-09 | 株式会社大和化成研究所 | Method for producing naphthalene aldehydes |
| GB9714275D0 (en) * | 1997-07-08 | 1997-09-10 | Ciba Geigy Ag | Oxidation process |
| US6616828B2 (en) * | 2001-08-06 | 2003-09-09 | Micron Technology, Inc. | Recovery method for platinum plating bath |
| WO2006054996A1 (en) * | 2004-11-19 | 2006-05-26 | Honeywell International Inc. | Selective removal chemistries for semiconductor applications, methods of production and uses thereof |
| JP5585980B2 (en) * | 2007-05-22 | 2014-09-10 | 奥野製薬工業株式会社 | Pretreatment method of electroless plating for resin molding, plating method for resin molding, and pretreatment agent |
| ES2334839T3 (en) * | 2007-08-10 | 2010-03-16 | Enthone Inc. | CHROME-FREE DECAPANT FOR PLASTIC SURFACES. |
| US8288030B2 (en) * | 2010-03-12 | 2012-10-16 | Sumitomo Electric Industries, Ltd. | Redox flow battery |
| US10260000B2 (en) * | 2012-01-23 | 2019-04-16 | Macdermid Acumen, Inc. | Etching of plastic using acidic solutions containing trivalent manganese |
| US8603352B1 (en) * | 2012-10-25 | 2013-12-10 | Rohm and Haas Electroncis Materials LLC | Chrome-free methods of etching organic polymers |
| PL2920341T3 (en) * | 2012-11-15 | 2019-05-31 | Macdermid Acumen Inc | Electrolytic generation of manganese (iii) ions in strong sulfuric acid |
-
2014
- 2014-03-07 WO PCT/US2014/021618 patent/WO2014164272A1/en not_active Ceased
- 2014-03-07 CA CA2901589A patent/CA2901589C/en active Active
- 2014-03-07 PL PL14779082T patent/PL2971260T3/en unknown
- 2014-03-07 AU AU2014249521A patent/AU2014249521B2/en active Active
- 2014-03-07 BR BR112015021067-8A patent/BR112015021067B1/en active IP Right Grant
- 2014-03-07 SI SI201431343T patent/SI2971260T1/en unknown
- 2014-03-07 CA CA2955467A patent/CA2955467C/en active Active
- 2014-03-07 MX MX2015012584A patent/MX379432B/en unknown
- 2014-03-07 JP JP2016500796A patent/JP6167222B2/en active Active
- 2014-03-07 LT LTEP14779082.8T patent/LT2971260T/en unknown
- 2014-03-07 PT PT14779082T patent/PT2971260T/en unknown
- 2014-03-07 ES ES14779082T patent/ES2745071T3/en active Active
- 2014-03-07 KR KR1020157028235A patent/KR101749947B1/en active Active
- 2014-03-07 EP EP14779082.8A patent/EP2971260B1/en active Active
- 2014-03-07 HR HRP20191626 patent/HRP20191626T1/en unknown
- 2014-03-07 CN CN201480014056.0A patent/CN105209667B/en active Active
- 2014-03-07 DK DK14779082.8T patent/DK2971260T3/en active
- 2014-03-07 HU HUE14779082A patent/HUE045344T2/en unknown
- 2014-03-11 TW TW103108294A patent/TWI489007B/en active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2971260A4 (en) | 2017-04-19 |
| BR112015021067A2 (en) | 2017-07-18 |
| SI2971260T1 (en) | 2019-12-31 |
| TWI489007B (en) | 2015-06-21 |
| TW201500593A (en) | 2015-01-01 |
| HRP20191626T1 (en) | 2019-12-13 |
| DK2971260T3 (en) | 2019-09-23 |
| MX379432B (en) | 2025-03-10 |
| KR20150126935A (en) | 2015-11-13 |
| CA2955467A1 (en) | 2014-10-09 |
| CA2901589A1 (en) | 2014-10-09 |
| PL2971260T3 (en) | 2020-03-31 |
| CA2901589C (en) | 2019-01-22 |
| ES2745071T3 (en) | 2020-02-27 |
| EP2971260A1 (en) | 2016-01-20 |
| WO2014164272A1 (en) | 2014-10-09 |
| CN105209667A (en) | 2015-12-30 |
| PT2971260T (en) | 2019-09-27 |
| EP2971260B1 (en) | 2019-06-19 |
| CA2955467C (en) | 2021-03-16 |
| KR101749947B1 (en) | 2017-06-22 |
| JP6167222B2 (en) | 2017-07-19 |
| JP2016512574A (en) | 2016-04-28 |
| BR112015021067B1 (en) | 2021-06-08 |
| LT2971260T (en) | 2019-09-25 |
| HUE045344T2 (en) | 2019-12-30 |
| CN105209667B (en) | 2017-12-05 |
| AU2014249521A1 (en) | 2015-08-27 |
| AU2014249521B2 (en) | 2018-03-01 |
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