MX2015007372A - Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas. - Google Patents
Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas.Info
- Publication number
- MX2015007372A MX2015007372A MX2015007372A MX2015007372A MX2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A MX 2015007372 A MX2015007372 A MX 2015007372A
- Authority
- MX
- Mexico
- Prior art keywords
- cyano
- methylsulfilimines
- pyridin
- ethyl
- preparation
- Prior art date
Links
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 title 1
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 abstract 4
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 abstract 2
- -1 Cyano-substituted sulfilimines Chemical class 0.000 abstract 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 150000003568 thioethers Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/57—Nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
- C07D213/32—Sulfur atoms
- C07D213/34—Sulfur atoms to which a second hetero atom is attached
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Las sulfiliminas ciano-substituidas se producen de forma eficaz y con alto rendimiento a partir de los correspondientes sulfuros, cianamida e hipoclorito mediante la adición del sulfuro a una solución de la cianamida e hipoclorito en presencia de un solvente de nitrilo mientras mantiene el pH de aproximadamente 8 a aproximadamente 12.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261735612P | 2012-12-11 | 2012-12-11 | |
| US201261735573P | 2012-12-11 | 2012-12-11 | |
| PCT/US2013/074006 WO2014093276A1 (en) | 2012-12-11 | 2013-12-10 | Improved process for the preparation of|n-cyano-s-[1 -(pyridin-3-yl)ethyl]-s-methylsulfilimines |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2015007372A true MX2015007372A (es) | 2015-09-23 |
Family
ID=49877060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2015007372A MX2015007372A (es) | 2012-12-11 | 2013-12-10 | Proceso mejorado para la preparacion de [n-ciano-s-[1-(piridin-3-i l) etil]-s-metilsulfiliminas. |
Country Status (14)
| Country | Link |
|---|---|
| US (2) | US20140163236A1 (es) |
| EP (1) | EP2931706A1 (es) |
| JP (1) | JP2016504304A (es) |
| KR (1) | KR20150092762A (es) |
| CN (1) | CN105324365A (es) |
| AR (1) | AR093901A1 (es) |
| AU (1) | AU2013359564A1 (es) |
| CA (1) | CA2894667A1 (es) |
| HK (1) | HK1214825A1 (es) |
| IL (1) | IL239228A0 (es) |
| MX (1) | MX2015007372A (es) |
| RU (1) | RU2015128003A (es) |
| WO (1) | WO2014093276A1 (es) |
| ZA (1) | ZA201503835B (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102064827B1 (ko) | 2012-02-16 | 2020-01-13 | 다우 아그로사이언시즈 엘엘씨 | 술필이민 화합물의 제조 방법 |
| TWI735573B (zh) * | 2016-06-21 | 2021-08-11 | 美商陶氏農業科學公司 | 生產某些經取代硫亞胺之方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2005310314B2 (en) | 2004-04-08 | 2011-07-21 | Corteva Agriscience Llc | Insecticidal N-substituted sulfoximines |
| TWI398433B (zh) | 2006-02-10 | 2013-06-11 | Dow Agrosciences Llc | 殺蟲性之n-取代(6-鹵烷基吡啶-3-基)烷基磺醯亞胺 |
| TWI381811B (zh) * | 2006-06-23 | 2013-01-11 | Dow Agrosciences Llc | 用以防治可抵抗一般殺蟲劑之昆蟲的方法 |
| CN101641331B (zh) * | 2007-02-26 | 2012-06-27 | 陶氏益农公司 | 制备某些取代的硫亚胺的方法 |
| KR102064827B1 (ko) * | 2012-02-16 | 2020-01-13 | 다우 아그로사이언시즈 엘엘씨 | 술필이민 화합물의 제조 방법 |
-
2013
- 2013-12-10 AR ARP130104608A patent/AR093901A1/es unknown
- 2013-12-10 CN CN201380064126.9A patent/CN105324365A/zh active Pending
- 2013-12-10 EP EP13811743.7A patent/EP2931706A1/en not_active Withdrawn
- 2013-12-10 RU RU2015128003A patent/RU2015128003A/ru not_active Application Discontinuation
- 2013-12-10 HK HK16102821.3A patent/HK1214825A1/zh unknown
- 2013-12-10 WO PCT/US2013/074006 patent/WO2014093276A1/en not_active Ceased
- 2013-12-10 US US14/101,536 patent/US20140163236A1/en not_active Abandoned
- 2013-12-10 AU AU2013359564A patent/AU2013359564A1/en not_active Abandoned
- 2013-12-10 CA CA2894667A patent/CA2894667A1/en not_active Abandoned
- 2013-12-10 KR KR1020157018301A patent/KR20150092762A/ko not_active Withdrawn
- 2013-12-10 MX MX2015007372A patent/MX2015007372A/es unknown
- 2013-12-10 JP JP2015545919A patent/JP2016504304A/ja active Pending
-
2015
- 2015-05-28 ZA ZA2015/03835A patent/ZA201503835B/en unknown
- 2015-06-04 IL IL239228A patent/IL239228A0/en unknown
-
2016
- 2016-01-19 US US15/000,623 patent/US20160137603A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| CN105324365A (zh) | 2016-02-10 |
| AU2013359564A1 (en) | 2015-06-11 |
| AR093901A1 (es) | 2015-06-24 |
| HK1214825A1 (zh) | 2016-08-05 |
| RU2015128003A (ru) | 2017-01-16 |
| ZA201503835B (en) | 2016-08-31 |
| IL239228A0 (en) | 2015-07-30 |
| KR20150092762A (ko) | 2015-08-13 |
| CA2894667A1 (en) | 2014-06-19 |
| WO2014093276A1 (en) | 2014-06-19 |
| JP2016504304A (ja) | 2016-02-12 |
| US20140163236A1 (en) | 2014-06-12 |
| EP2931706A1 (en) | 2015-10-21 |
| US20160137603A1 (en) | 2016-05-19 |
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