MX2014001605A - Proceso para la preparacion de compuestos de cloruro de 1h - pirazol - 5 - carbonilo n - sustituidos. - Google Patents
Proceso para la preparacion de compuestos de cloruro de 1h - pirazol - 5 - carbonilo n - sustituidos.Info
- Publication number
- MX2014001605A MX2014001605A MX2014001605A MX2014001605A MX2014001605A MX 2014001605 A MX2014001605 A MX 2014001605A MX 2014001605 A MX2014001605 A MX 2014001605A MX 2014001605 A MX2014001605 A MX 2014001605A MX 2014001605 A MX2014001605 A MX 2014001605A
- Authority
- MX
- Mexico
- Prior art keywords
- pyrazole
- preparing
- formula
- compound
- carbonylchlorid
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- ZLIZZDCWMOGEGA-UHFFFAOYSA-N 1h-pyrazole-5-carbonyl chloride Chemical class ClC(=O)C=1C=CNN=1 ZLIZZDCWMOGEGA-UHFFFAOYSA-N 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- -1 1 H-pyrazole-5-carbonylchloride compound Chemical class 0.000 abstract 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 229910052744 lithium Inorganic materials 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 239000011777 magnesium Substances 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/04—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
La presente invención se refiere a un proceso para la preparación de un compuesto de cloruro de 1H-pirazol-5-carbonilo N-sustituido de la fórmula (I) (ver Fórmula) en la cual R1 es hidrógeno, halógeno, ciano, alquilo C1-C6, fluoroalquilo C1-C6, cicloalquilo C3-C8, fluorocicloalquilo C3-C8, alquenilo C2-C6, fluoroalquenilo C2-C6, alcoxi C1-C6, fluoroalcoxi C1-C6, fluoroalcoxi C1-C4-alquilo C1-C4, fenilo y similares; cada R2 se selecciona en forma independiente de halógeno, alquilo C1-C6, fluoroalquilo C1-C6, cicloalquilo C3-C8, fluorocicloalquilo C3-C8, alquenilo C2-C6, fluoroalquenilo C2-C6, alcoxi C1-C6, fenilo y similares; r es 0, 1, 2, 3 o 4; que comprenden los pasos de i) desprotonar un compuesto de la fórmula (II) (ver Fórmula) en la cual las variables R1, R2 y r son cada una como se definió con anterioridad, con una base seleccionada de base orgánica de litio que tiene un litio unido a carbono o nitrógeno o con una base orgánica de magnesio que tiene un magnesio unido a carbono; y ii) someter el producto obtenido en el paso (i) a clorocarbonilación por medio de su reacción con un reactivo seleccionado del grupo que consiste un fosgeno o un equivalente de fosgeno, para obtener un compuesto de la fórmula (I).
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161522746P | 2011-08-12 | 2011-08-12 | |
| EP11177494 | 2011-08-12 | ||
| PCT/EP2012/065648 WO2013024007A1 (en) | 2011-08-12 | 2012-08-10 | Process for preparing n-substituted 1h-pyrazole-5-carbonylchloride compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2014001605A true MX2014001605A (es) | 2014-05-01 |
Family
ID=47714794
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014001605A MX2014001605A (es) | 2011-08-12 | 2012-08-10 | Proceso para la preparacion de compuestos de cloruro de 1h - pirazol - 5 - carbonilo n - sustituidos. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8921567B2 (es) |
| EP (1) | EP2742035A1 (es) |
| JP (1) | JP5955961B2 (es) |
| KR (1) | KR20140051401A (es) |
| CN (1) | CN103874694B (es) |
| AU (1) | AU2012297002A1 (es) |
| BR (1) | BR112014003111A2 (es) |
| IL (1) | IL230594A (es) |
| MX (1) | MX2014001605A (es) |
| WO (1) | WO2013024007A1 (es) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101335224B1 (ko) | 2005-07-07 | 2013-11-29 | 바스프 에스이 | Ｎ-티오안트라닐아미드 화합물 및 살충제로서의 이의 용도 |
| KR20140064849A (ko) | 2011-08-12 | 2014-05-28 | 바스프 에스이 | 아닐린 유형 화합물 |
| BR112014003111A2 (pt) | 2011-08-12 | 2017-02-21 | Basf Se | processo para preparar um composto de 1h-pirazol-5- carbonilcloreto n-substituído e processo para preparar um composto de sulfimina |
| MX2014001609A (es) | 2011-08-12 | 2014-05-01 | Basf Se | Compuestos de n-tio-antranilamida y sus usos como plaguicidas. |
| AU2012342564A1 (en) | 2011-11-21 | 2014-06-12 | Basf Se | Process for preparing N-substituted 1H-pyrazole-5-carboxylate compounds and derivatives thereof |
| AU2013265512A1 (en) | 2012-05-24 | 2014-12-18 | Basf Se | N-thio-anthranilamide compounds and their use as pesticides |
| ES2618257T3 (es) | 2012-08-17 | 2017-06-21 | Basf Se | Carbamato-benzoxazinonas útiles para preparar triazin-benzoxazinonas |
| WO2014079820A1 (en) | 2012-11-22 | 2014-05-30 | Basf Se | Use of anthranilamide compounds for reducing insect-vectored viral infections |
| EP2978315A1 (en) * | 2013-03-28 | 2016-02-03 | Basf Se | Process for preparing sulfimines and their in-situ conversion into n-(2-amino-benzoyl)-sulfimines |
| JP2016518433A (ja) * | 2013-05-17 | 2016-06-23 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | Ｎ置換１ｈ−ピラゾール−５−カルボン酸化合物及びその誘導体を製造する方法 |
| EP3010898A1 (en) * | 2013-06-20 | 2016-04-27 | Basf Se | Process for preparing pyridylpyrazole compounds and derivatives thereof from pyridylhydrazine |
| WO2016091674A1 (en) | 2014-12-12 | 2016-06-16 | Basf Se | Use of cyclaniliprole on cultivated plants |
| MX2018010011A (es) | 2016-02-19 | 2018-11-09 | Basf Se | Mezclas activas para uso pesticida que comprenden compuestos de antranilamida. |
| AU2019387370A1 (en) | 2018-11-30 | 2021-06-10 | Nuvation Bio Inc. | Pyrrole and pyrazole compounds and methods of use thereof |
| TW202241859A (zh) * | 2021-01-29 | 2022-11-01 | 美商富曼西公司 | 用於製備５－溴－２－（３－氯－吡啶－２－基）－２ｈ－吡唑－３－甲酸之方法 |
| CN119056375B (zh) * | 2024-11-05 | 2025-03-07 | 天津凯莱英医药科技发展有限公司 | 氟唑菌酰胺制备方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6136983A (en) | 1995-06-05 | 2000-10-24 | Rhone-Poulenc Agrochimie | Pesticidal sulfur compounds |
| MY138097A (en) | 2000-03-22 | 2009-04-30 | Du Pont | Insecticidal anthranilamides |
| CN100352808C (zh) | 2001-03-05 | 2007-12-05 | 杜邦公司 | 杂环二酰胺无脊椎害虫控制剂 |
| MY142967A (en) | 2001-08-13 | 2011-01-31 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
| AR036872A1 (es) | 2001-08-13 | 2004-10-13 | Du Pont | Compuesto de antranilamida, composicion que lo comprende y metodo para controlar una plaga de invertebrados |
| CN1865258A (zh) | 2001-08-15 | 2006-11-22 | 纳幕尔杜邦公司 | 用于控制无脊椎害虫的邻位取代的芳基酰胺化合物 |
| ATE417829T1 (de) | 2001-08-16 | 2009-01-15 | Du Pont | Substituierte anthranilamide und ihre verwendung als pesticide |
| TW200724033A (en) | 2001-09-21 | 2007-07-01 | Du Pont | Anthranilamide arthropodicide treatment |
| WO2008011131A2 (en) | 2006-07-21 | 2008-01-24 | Takeda Pharmaceutical Company Limited | Amide compounds |
| CN100335477C (zh) | 2002-06-13 | 2007-09-05 | 纳幕尔杜邦公司 | 吡唑甲酰胺杀虫剂 |
| TWI326283B (en) * | 2002-07-31 | 2010-06-21 | Du Pont | Method for preparing fused oxazinones |
| DE102004031100A1 (de) | 2004-06-28 | 2006-01-12 | Bayer Cropscience Ag | Anthranilamide |
| MY140912A (en) | 2004-07-26 | 2010-01-29 | Du Pont | Mixtures of anthranilamide invertebrate pest control agents |
| TWI363756B (en) | 2004-12-07 | 2012-05-11 | Du Pont | Method for preparing n-phenylpyrazole-1-carboxamides |
| KR101335224B1 (ko) | 2005-07-07 | 2013-11-29 | 바스프 에스이 | Ｎ-티오안트라닐아미드 화합물 및 살충제로서의 이의 용도 |
| US7867949B2 (en) | 2005-10-14 | 2011-01-11 | Sumitomo Chemical Company, Limited | Hydrazide compound and pesticidal use of the same |
| JP5186751B2 (ja) * | 2005-10-14 | 2013-04-24 | 住友化学株式会社 | ヒドラジド化合物およびその有害生物防除用途 |
| HUP0600573A2 (en) | 2006-07-12 | 2008-06-30 | Laszlo Pirity | Multifunction safety foil, especially fire-prevention foil |
| CL2008000979A1 (es) | 2007-04-11 | 2008-10-17 | Sumitomo Chemical Co | Proceso para producir un compuesto derivado de 2-piridin-2-il-2h-pirazol-3-fenilamida; compuestos intermediarios; el compuesto en si; composicion plaguicida que contiene a dicho compuesto; uso de dicho compuesto como plaguicida; y metodo para control |
| JP2008280336A (ja) | 2007-04-11 | 2008-11-20 | Sumitomo Chemical Co Ltd | アミド化合物の製造方法 |
| JP2008280341A (ja) | 2007-04-12 | 2008-11-20 | Sumitomo Chemical Co Ltd | ヒドラジド化合物およびその防除用途 |
| WO2008141843A1 (en) | 2007-05-24 | 2008-11-27 | Bayer Schering Pharma Aktiengesellschaft | Novel sulphoximine-substituted quinazoline and quinazoline derivatives as kinase inhibitors |
| TWI431000B (zh) | 2008-03-05 | 2014-03-21 | Du Pont | 製備２－胺基－５－氰基苯甲酸衍生物之方法 |
| WO2011064188A1 (en) | 2009-11-27 | 2011-06-03 | Basf Se | Insecticidal methods using nitrogen-containing heteroaromatic compounds |
| IN2014CN01025A (es) | 2011-08-12 | 2015-04-10 | Basf Se | |
| KR20140064849A (ko) | 2011-08-12 | 2014-05-28 | 바스프 에스이 | 아닐린 유형 화합물 |
| BR112014003111A2 (pt) | 2011-08-12 | 2017-02-21 | Basf Se | processo para preparar um composto de 1h-pirazol-5- carbonilcloreto n-substituído e processo para preparar um composto de sulfimina |
| MX2014001609A (es) | 2011-08-12 | 2014-05-01 | Basf Se | Compuestos de n-tio-antranilamida y sus usos como plaguicidas. |
| AU2012342564A1 (en) | 2011-11-21 | 2014-06-12 | Basf Se | Process for preparing N-substituted 1H-pyrazole-5-carboxylate compounds and derivatives thereof |
-
2012
- 2012-08-10 BR BR112014003111A patent/BR112014003111A2/pt not_active IP Right Cessation
- 2012-08-10 US US14/235,556 patent/US8921567B2/en not_active Expired - Fee Related
- 2012-08-10 JP JP2014524392A patent/JP5955961B2/ja not_active Expired - Fee Related
- 2012-08-10 AU AU2012297002A patent/AU2012297002A1/en not_active Abandoned
- 2012-08-10 KR KR1020147006251A patent/KR20140051401A/ko not_active Withdrawn
- 2012-08-10 EP EP12744006.3A patent/EP2742035A1/en not_active Withdrawn
- 2012-08-10 WO PCT/EP2012/065648 patent/WO2013024007A1/en not_active Ceased
- 2012-08-10 MX MX2014001605A patent/MX2014001605A/es unknown
- 2012-08-10 CN CN201280050055.2A patent/CN103874694B/zh not_active Expired - Fee Related
-
2014
- 2014-01-22 IL IL230594A patent/IL230594A/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| US8921567B2 (en) | 2014-12-30 |
| AU2012297002A1 (en) | 2014-03-06 |
| BR112014003111A2 (pt) | 2017-02-21 |
| EP2742035A1 (en) | 2014-06-18 |
| JP2014521712A (ja) | 2014-08-28 |
| KR20140051401A (ko) | 2014-04-30 |
| IL230594A0 (en) | 2014-03-31 |
| JP5955961B2 (ja) | 2016-07-20 |
| IL230594A (en) | 2016-11-30 |
| CN103874694A (zh) | 2014-06-18 |
| WO2013024007A1 (en) | 2013-02-21 |
| CN103874694B (zh) | 2016-08-17 |
| US20140163234A1 (en) | 2014-06-12 |
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