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MX2013013379A - Metodo para capturar y reciclar catalizador de hierro utilizado en la produccion de compuestos de haloalcano. - Google Patents

Metodo para capturar y reciclar catalizador de hierro utilizado en la produccion de compuestos de haloalcano.

Info

Publication number
MX2013013379A
MX2013013379A MX2013013379A MX2013013379A MX2013013379A MX 2013013379 A MX2013013379 A MX 2013013379A MX 2013013379 A MX2013013379 A MX 2013013379A MX 2013013379 A MX2013013379 A MX 2013013379A MX 2013013379 A MX2013013379 A MX 2013013379A
Authority
MX
Mexico
Prior art keywords
production
hcc
capturing
catalyst used
iron catalyst
Prior art date
Application number
MX2013013379A
Other languages
English (en)
Other versions
MX362213B (es
Inventor
Stephen A Cottrell
Hsueh Sung Tung
Joshua Close
Haiyou Wang
Original Assignee
Honeywell Int Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Honeywell Int Inc filed Critical Honeywell Int Inc
Publication of MX2013013379A publication Critical patent/MX2013013379A/es
Publication of MX362213B publication Critical patent/MX362213B/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/0075—Separating solid material from the gas/liquid stream by electrostatic precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C1/00—Magnetic separation
    • B03C1/02—Magnetic separation acting directly on the substance being separated
    • B03C1/025—High gradient magnetic separators
    • B03C1/031—Component parts; Auxiliary operations
    • B03C1/033—Component parts; Auxiliary operations characterised by the magnetic circuit
    • B03C1/0335—Component parts; Auxiliary operations characterised by the magnetic circuit using coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C5/00—Separating dispersed particles from liquids by electrostatic effect
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04—Chloro-alkenes
    • C07C21/06—Vinyl chloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C2201/00—Details of magnetic or electrostatic separation
    • B03C2201/02—Electrostatic separation of liquids from liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C—MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03C2201/00—Details of magnetic or electrostatic separation
    • B03C2201/18—Magnetic separation whereby the particles are suspended in a liquid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

Se da a conocer un método para la captura y el reciclaje de catalizador de hierro utilizado en la producción de compuestos de haloalcano y, más particularmente, a un procedimiento mejorado para la fabricación del compuesto de 1,1,1,3,3-pentacloropropano (HCC-240fa), en donde una unidad de separación electromagnética (EMSU) se utiliza para facilitar la reacción. Cuando se activa, las funciones EMSU para eliminar las partículas de hierro desde el efluente del reactor; sin corriente, las partículas de hierro capturados por el EMSU se pueden lavar de nuevo en el reactor para su reutilización en la producción continua de HCC-240fa. La presente invención también es útil en los procesos de fabricación de otros compuestos tales como haloalcano HCC-250 y HCC-360.
MX2013013379A 2011-06-03 2012-05-31 Metodo para capturar y reciclar catalizador de hierro utilizado en la produccion de compuestos de haloalcano. MX362213B (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161492907P 2011-06-03 2011-06-03
US13/471,601 US10112166B2 (en) 2011-06-03 2012-05-15 Method for capturing and recycling iron catalyst used in the production of haloalkane compounds
PCT/US2012/040070 WO2012166836A2 (en) 2011-06-03 2012-05-31 Method for capturing and recycling iron catalyst used in the production of haloalkane compounds

Publications (2)

Publication Number Publication Date
MX2013013379A true MX2013013379A (es) 2013-12-02
MX362213B MX362213B (es) 2019-01-09

Family

ID=47260294

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2013013379A MX362213B (es) 2011-06-03 2012-05-31 Metodo para capturar y reciclar catalizador de hierro utilizado en la produccion de compuestos de haloalcano.

Country Status (10)

Country Link
US (1) US10112166B2 (es)
EP (1) EP2714270B1 (es)
JP (2) JP6152097B2 (es)
KR (1) KR102002932B1 (es)
CN (2) CN109127146A (es)
CA (1) CA2836077A1 (es)
ES (1) ES2674283T3 (es)
MX (1) MX362213B (es)
RU (1) RU2606633C2 (es)
WO (1) WO2012166836A2 (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8859829B2 (en) * 2013-03-14 2014-10-14 Honeywell International Inc. Stabilizer and inhibitor for chloropropenes, such as tetrachloropropene 1,1,2,3-tetrachloropropene (1230xa), used in the manufacture of 2,3,3,3-tetrafluoropropene (1234yf)
US9090531B2 (en) * 2013-03-14 2015-07-28 Honeywell International Inc. Method for mitigating HCL generation during 1,1,2,3-tetrachloropropene purification
US10717662B2 (en) * 2018-02-07 2020-07-21 Honeywell International Inc. Process for the removal of iron and phosphate ions from a chlorinated hydrocarbon waste stream
CN111902384B (zh) * 2018-04-03 2024-05-14 蓝立方知识产权有限责任公司 在氯化烷烃生产中回收催化剂的方法
CN111659322A (zh) * 2019-03-06 2020-09-15 浙江佳汇新材料有限公司 一种制备1,1,1,3-四氯丙烷的装置及工艺

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EP0014802B1 (en) * 1978-12-21 1984-03-21 Imperial Chemical Industries Plc Liquid phase chemical process with separation of catalyst particles by magnetic flocculation
US4605678A (en) * 1984-03-12 1986-08-12 Mobil Oil Corporation Separation of catalyst from slurry bubble column wax and catalyst recycle
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JPH0356153A (ja) 1989-07-25 1991-03-11 Tadahiko Yokoe 自動脱鉄装置
JPH06170245A (ja) * 1992-12-02 1994-06-21 Tdk Corp 磁性触媒粒子の回収方法
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US6235951B1 (en) 1996-01-17 2001-05-22 Central Glass Company, Limited Method for producing 1,1,1,3,3-pentafluoropropane
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US6313360B1 (en) * 2000-09-29 2001-11-06 Vulcan Materials Company Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
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CN2535130Y (zh) 2002-03-15 2003-02-12 河北科技大学 一种电磁分离器
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Also Published As

Publication number Publication date
US10112166B2 (en) 2018-10-30
KR102002932B1 (ko) 2019-07-23
RU2606633C2 (ru) 2017-01-10
KR20140037151A (ko) 2014-03-26
EP2714270A4 (en) 2015-03-11
ES2674283T3 (es) 2018-06-28
WO2012166836A2 (en) 2012-12-06
JP2014527458A (ja) 2014-10-16
EP2714270B1 (en) 2018-03-21
MX362213B (es) 2019-01-09
CN109127146A (zh) 2019-01-04
JP2017127870A (ja) 2017-07-27
WO2012166836A3 (en) 2013-03-21
CA2836077A1 (en) 2012-12-06
US20120305454A1 (en) 2012-12-06
EP2714270A2 (en) 2014-04-09
RU2013156262A (ru) 2015-07-20
CN103648640A (zh) 2014-03-19
JP6152097B2 (ja) 2017-06-21

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