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MX2011011732A - Metodo continuo para producir esteres de acidos carboxilicos alifaticos. - Google Patents

Metodo continuo para producir esteres de acidos carboxilicos alifaticos.

Info

Publication number
MX2011011732A
MX2011011732A MX2011011732A MX2011011732A MX2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A
Authority
MX
Mexico
Prior art keywords
continuous method
aliphatic carboxylic
carboxylic acids
optionally substituted
formula
Prior art date
Application number
MX2011011732A
Other languages
English (en)
Inventor
Roman Morschhaeuser
Matthias Krull
Original Assignee
Clariant Finance Bvi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Clariant Finance Bvi Ltd filed Critical Clariant Finance Bvi Ltd
Publication of MX2011011732A publication Critical patent/MX2011011732A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122—Incoherent waves
    • B01J19/126—Microwaves
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00—Heating by electric, magnetic or electromagnetic fields
    • H05B6/64—Heating using microwaves
    • H05B6/70—Feed lines
    • H05B6/701—Feed lines using microwave applicators
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00—Heating by electric, magnetic or electromagnetic fields
    • H05B6/64—Heating using microwaves
    • H05B6/80—Apparatus for specific applications
    • H05B6/806—Apparatus for specific applications for laboratory use
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1209—Features relating to the reactor or vessel
    • B01J2219/1212—Arrangements of the reactor or the reactors
    • B01J2219/1215—Single reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1209—Features relating to the reactor or vessel
    • B01J2219/1221—Features relating to the reactor or vessel the reactor per se
    • B01J2219/1224—Form of the reactor
    • B01J2219/1227—Reactors comprising tubes with open ends
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1248—Features relating to the microwave cavity
    • B01J2219/1272—Materials of construction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1275—Controlling the microwave irradiation variables
    • B01J2219/1281—Frequency
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1275—Controlling the microwave irradiation variables
    • B01J2219/1284—Intensity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1287—Features relating to the microwave source
    • B01J2219/129—Arrangements thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Clinical Laboratory Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La invención se refiere a un método continuo para producir ésteres de ácido carbónico alifáticos haciendo reaccionar por lo menos un ácido carboxulico alifático de la fórmula (l):R1-COOH (I), en donde R1 representa hidrógeno o un grupo hidrocarburo alifático opcionalmente sustituido con de 1 a 50 átomos de carbono, con por lo menos un alcohol de la fórmula (Il):R2-(OH)n(ll), en donde: R2representa un grupo hidrocarburo opcionalmente sustituido con de 1 a 100 átomos de carbono y n es un número entero de 1 a 10, en la presencia de por lo menos un catalizador de transesterificación en un tubo de reacción, el eje longitudinal del mismo se extiende en la dirección de propagación de las microondas de un aplicador de microondas de monomodo, bajo radiación de microondas para formar el éster.
MX2011011732A 2009-06-30 2010-06-09 Metodo continuo para producir esteres de acidos carboxilicos alifaticos. MX2011011732A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009031053A DE102009031053A1 (de) 2009-06-30 2009-06-30 Kontinuierliches Verfahren zur Herstellung von Estern aliphatischer Carbonsäuren
PCT/EP2010/003446 WO2011000463A2 (de) 2009-06-30 2010-06-09 Kontinuierliches verfahren zur herstellung von estern aliphatischer carbonsäuren

Publications (1)

Publication Number Publication Date
MX2011011732A true MX2011011732A (es) 2011-11-29

Family

ID=43128288

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2011011732A MX2011011732A (es) 2009-06-30 2010-06-09 Metodo continuo para producir esteres de acidos carboxilicos alifaticos.

Country Status (14)

Country Link
US (1) US20120103790A1 (es)
EP (1) EP2448905B1 (es)
JP (2) JP5961552B2 (es)
KR (1) KR20120046720A (es)
CN (1) CN102741212B (es)
AU (2) AU2010268448A1 (es)
BR (1) BRPI1012744A2 (es)
CA (1) CA2766952A1 (es)
DE (1) DE102009031053A1 (es)
EA (1) EA021516B1 (es)
ES (1) ES2405687T3 (es)
MX (1) MX2011011732A (es)
MY (1) MY152089A (es)
WO (1) WO2011000463A2 (es)

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DE102008017218B4 (de) * 2008-04-04 2011-09-22 Clariant International Ltd. Kontinuierliches Verfahren zur Herstellung von Amiden niederer aliphatischer Carbonsäuren
DE102008017213B4 (de) * 2008-04-04 2012-08-09 Clariant International Limited Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren
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Also Published As

Publication number Publication date
AU2016203660A1 (en) 2016-07-28
ES2405687T3 (es) 2013-06-03
JP2012531452A (ja) 2012-12-10
WO2011000463A3 (de) 2011-03-31
EA021516B1 (ru) 2015-07-30
KR20120046720A (ko) 2012-05-10
WO2011000463A2 (de) 2011-01-06
CN102741212B (zh) 2014-12-10
JP5961552B2 (ja) 2016-08-02
US20120103790A1 (en) 2012-05-03
JP2016138123A (ja) 2016-08-04
BRPI1012744A2 (pt) 2016-03-22
EP2448905A2 (de) 2012-05-09
EP2448905B1 (de) 2013-04-17
MY152089A (en) 2014-08-15
CN102741212A (zh) 2012-10-17
EA201200069A1 (ru) 2012-05-30
AU2010268448A1 (en) 2011-11-03
DE102009031053A1 (de) 2011-01-13
CA2766952A1 (en) 2011-01-06

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