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MX2011008931A - Un proceso para la preparacion eco-amigable de 3,5-dibromo-4-hidroxibenzonitrilo. - Google Patents

Un proceso para la preparacion eco-amigable de 3,5-dibromo-4-hidroxibenzonitrilo.

Info

Publication number
MX2011008931A
MX2011008931A MX2011008931A MX2011008931A MX2011008931A MX 2011008931 A MX2011008931 A MX 2011008931A MX 2011008931 A MX2011008931 A MX 2011008931A MX 2011008931 A MX2011008931 A MX 2011008931A MX 2011008931 A MX2011008931 A MX 2011008931A
Authority
MX
Mexico
Prior art keywords
hydroxybenzonitrile
dibromo
eco
friendly preparation
friendly
Prior art date
Application number
MX2011008931A
Other languages
English (en)
Inventor
Subbarayappa Adimurthy
Gadde Ramachandraiah
Girdhar Joshi
Rajendra Patil
Maheshkumar Ramniklal Gandhi
Mallampati Subbareddy
Pratyush Maiti
Original Assignee
Council Of Scient & Ind Res An Indian Registered Body Inc Under The Registration Of Societes Act Act
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Council Of Scient & Ind Res An Indian Registered Body Inc Under The Registration Of Societes Act Act filed Critical Council Of Scient & Ind Res An Indian Registered Body Inc Under The Registration Of Societes Act Act
Publication of MX2011008931A publication Critical patent/MX2011008931A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
    • B01J31/2208—Oxygen, e.g. acetylacetonates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/49—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C255/53—Carboxylic acid nitriles having cyano groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton containing cyano groups and hydroxy groups bound to the carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Un 3, 5-dibromo-4-hidroxibenzonitrilo (bromoxinilo) bastante puro se ha preparado en alto rendimiento a partir de 4-hidroxibenzonitrilo utilizando un reactivo de bromación sin daño ecológico que comprende una proporción molar 2:1 de bromuro para sales de bromato en medio ácido acuoso sin ningún catalizador bajo condiciones ambientales sin ningún procedimiento de preparación. El producto 3,5-dibromo-4-hidroxibenzonitrilo se obtuvo en un rendimiento del 91-99% con un punto de fusión de 189-191°C y más del 99 de pureza mediante un análisis cromatográfico gaseoso sin ninguna purificación.
MX2011008931A 2009-02-25 2010-02-25 Un proceso para la preparacion eco-amigable de 3,5-dibromo-4-hidroxibenzonitrilo. MX2011008931A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IN349DE2009 2009-02-25
PCT/IN2010/000111 WO2010097812A1 (en) 2009-02-25 2010-02-25 A process for the eco-friendly preparation of 3, 5-dibromo-4-hydroxybenzonitrile

Publications (1)

Publication Number Publication Date
MX2011008931A true MX2011008931A (es) 2012-02-28

Family

ID=42201031

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2011008931A MX2011008931A (es) 2009-02-25 2010-02-25 Un proceso para la preparacion eco-amigable de 3,5-dibromo-4-hidroxibenzonitrilo.

Country Status (11)

Country Link
US (1) US8957239B2 (es)
EP (1) EP2408736B1 (es)
JP (1) JP5680561B2 (es)
KR (1) KR20110120332A (es)
CN (1) CN102333758B (es)
AU (1) AU2010217236B2 (es)
CA (1) CA2753644C (es)
ES (1) ES2471365T3 (es)
IL (1) IL214786A (es)
MX (1) MX2011008931A (es)
WO (1) WO2010097812A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105859583B (zh) * 2016-05-11 2018-01-16 衢州英特高分子材料有限公司 一种2,6‑二溴‑4‑氰基苯酚的合成方法
CN108129351A (zh) * 2017-12-27 2018-06-08 安徽太主科技发展有限公司 一种4′-溴甲基-2-氰基联苯的制备方法
CN109212069B (zh) * 2018-09-24 2021-05-07 丁立平 一种测定玉米和小麦中痕量溴苯腈、碘苯腈和羟敌草腈残留量的气相色谱法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2095275A (en) * 1935-05-27 1937-10-12 Dow Chemical Co Preparation of 1,3-dihalo-and 1,3,5-trihalobenzenes
US2979537A (en) * 1959-02-04 1961-04-11 Dow Chemical Co Selective bromination of benzene
US3062899A (en) * 1960-06-17 1962-11-06 Shell Oil Co Halogenation process
FR1375311A (fr) * 1962-09-24 1964-10-16 May & Baker Ltd Nouvelles compositions herbicides à base de dérivés du benzonitrile
US4349488A (en) * 1981-11-03 1982-09-14 Great Lakes Chemical Corporation Process for producing esters of 3,5-dibromo-4-hydroxybenzonitrile
US4436665A (en) * 1982-09-29 1984-03-13 Union Carbide Corporation Two solvent process for preparation of esters of 3,5-dibromo-4-hydroxybenzonitrile
DE3561389D1 (en) * 1984-03-07 1988-02-18 Ihara Chemical Ind Co Process for producing a halobenzene
DE3431826A1 (de) * 1984-08-30 1986-03-13 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung aromatischer bromverbindungen
JPH03115253A (ja) * 1989-09-28 1991-05-16 Nippon Shirika Kogyo Kk 多臭素化第４アンモニウム塩の製造方法
IL148144A0 (en) * 2001-01-22 2002-12-01 Council Scient Ind Res An eco-friendly method of preparation of high purity tetrabromobisphenol-a
US6740253B2 (en) * 2002-01-23 2004-05-25 Council Of Scientific And Industrial Research Preparation of non-hazardous brominating reagents
MXPA04007215A (es) * 2002-01-25 2004-11-26 Council Of Scietific And Ind R Preparacion de reactivos de bromacion no peligrosos.
CN100425527C (zh) * 2003-05-30 2008-10-15 科学与工业研究委员会 制备无害的溴化试剂的方法
EP1697286B1 (en) * 2003-12-15 2009-08-26 Council of Scientific and Industrial Research A process for eco-friendly synthesis of bromobenzene
US8389719B2 (en) * 2005-06-10 2013-03-05 Ciba Specialty Chemicals Corp. Hydroxyphenyltriazines with an aromatic carbocyclic fused ring system

Also Published As

Publication number Publication date
ES2471365T3 (es) 2014-06-26
IL214786A0 (en) 2011-10-31
CA2753644A1 (en) 2010-09-02
AU2010217236A8 (en) 2014-10-23
AU2010217236A1 (en) 2011-09-15
IL214786A (en) 2014-11-30
AU2010217236B2 (en) 2014-10-30
CN102333758B (zh) 2014-04-02
US20130331596A1 (en) 2013-12-12
WO2010097812A1 (en) 2010-09-02
US8957239B2 (en) 2015-02-17
EP2408736B1 (en) 2014-04-30
KR20110120332A (ko) 2011-11-03
CA2753644C (en) 2017-01-03
JP2012518682A (ja) 2012-08-16
EP2408736A1 (en) 2012-01-25
JP5680561B2 (ja) 2015-03-04
CN102333758A (zh) 2012-01-25

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