MX2010001191A - Procedimeinto para la produccion de un compuesto de toluidina. - Google Patents
Procedimeinto para la produccion de un compuesto de toluidina.Info
- Publication number
- MX2010001191A MX2010001191A MX2010001191A MX2010001191A MX2010001191A MX 2010001191 A MX2010001191 A MX 2010001191A MX 2010001191 A MX2010001191 A MX 2010001191A MX 2010001191 A MX2010001191 A MX 2010001191A MX 2010001191 A MX2010001191 A MX 2010001191A
- Authority
- MX
- Mexico
- Prior art keywords
- reaction
- solvent
- product
- fluazinam
- simple operations
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- -1 toluidine compound Chemical class 0.000 title 1
- 239000005780 Fluazinam Substances 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 2
- UZCGKGPEKUCDTF-UHFFFAOYSA-N fluazinam Chemical compound [O-][N+](=O)C1=CC(C(F)(F)F)=C(Cl)C([N+]([O-])=O)=C1NC1=NC=C(C(F)(F)F)C=C1Cl UZCGKGPEKUCDTF-UHFFFAOYSA-N 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000004480 active ingredient Substances 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000007810 chemical reaction solvent Substances 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 150000002825 nitriles Chemical class 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/72—Nitrogen atoms
- C07D213/74—Amino or imino radicals substituted by hydrocarbon or substituted hydrocarbon radicals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pyridine Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Abstract
Debido a que el fluazinam es excelente como ingrediente activo de plaguicidas y sumamente útil, es deseable producirlo de modo eficiente en una forma apropiada con operaciones simples a bajo costo de un modo que no perjudique el medio ambiente; el producto deseado se obtiene en buenos rendimientos con operaciones simples mediante fa utilización de sistemas de reacción ventajosos desde el punto de vista industrial a través de un procedimiento que comprende (1) una etapa de hacer reaccionar ACTF y DCDNBTF en presencia de un componente alcalino, un solvente seleccionado del grupo integrado por cetonas, nitrilos, éteres y ésteres y una cantidad suficiente de agua para disolver sustancialmente el componente alcalino, (2) una etapa de neutralización o acidificación de la mezcla de reacción con un ácido y (3) una etapa de remoción del solvente mediante destilación de la mezcla que contiene fluazinam como el producto de reacción y el solvente de la reacción para precipitar cristales del producto.
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007202220 | 2007-08-02 | ||
| JP2007202210 | 2007-08-02 | ||
| JP2007266000 | 2007-10-12 | ||
| JP2008037841 | 2008-02-19 | ||
| PCT/JP2008/063933 WO2009017241A2 (en) | 2007-08-02 | 2008-07-29 | Process for producing toluidine compound |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2010001191A true MX2010001191A (es) | 2010-03-01 |
Family
ID=40120103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2010001191A MX2010001191A (es) | 2007-08-02 | 2008-07-29 | Procedimeinto para la produccion de un compuesto de toluidina. |
Country Status (25)
| Country | Link |
|---|---|
| US (1) | US8338612B2 (es) |
| EP (1) | EP2170829B1 (es) |
| JP (1) | JP5390800B2 (es) |
| KR (1) | KR101461259B1 (es) |
| CN (1) | CN101778824B (es) |
| AR (1) | AR068801A1 (es) |
| AU (1) | AU2008283242B2 (es) |
| BR (1) | BRPI0814887B1 (es) |
| CA (1) | CA2694939C (es) |
| CL (1) | CL2008002275A1 (es) |
| DK (1) | DK2170829T3 (es) |
| ES (1) | ES2503541T3 (es) |
| GE (1) | GEP20135742B (es) |
| HR (1) | HRP20140960T1 (es) |
| IL (1) | IL203608A (es) |
| MX (1) | MX2010001191A (es) |
| NZ (1) | NZ582589A (es) |
| PL (1) | PL2170829T3 (es) |
| PT (1) | PT2170829E (es) |
| RS (1) | RS53735B1 (es) |
| RU (1) | RU2470919C2 (es) |
| SI (1) | SI2170829T1 (es) |
| TW (1) | TWI417285B (es) |
| WO (1) | WO2009017241A2 (es) |
| ZA (1) | ZA201000670B (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NZ600896A (en) | 2005-11-23 | 2013-12-20 | Makhteshim Chem Works Ltd | Process for preparing pyridinamines and novel polymorphs thereof |
| ITBS20100012A1 (it) * | 2010-01-28 | 2011-07-29 | Finchimica Srl | Procedimento per la preparazione di fluazinam |
| CN103626695B (zh) * | 2013-12-04 | 2015-04-22 | 泰州百力化学股份有限公司 | 一种以混合溶剂为介质制备氟啶胺的新方法 |
| CN106316937A (zh) * | 2015-06-29 | 2017-01-11 | 江苏威耳化工有限公司 | 一种氟啶胺的制备方法 |
| CN109988103A (zh) * | 2017-12-29 | 2019-07-09 | 江苏扬农化工股份有限公司 | 一种合成氟啶胺的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6052146B2 (ja) * | 1979-12-25 | 1985-11-18 | 石原産業株式会社 | Ｎ−ピリジルアニリン系化合物、それらの製造方法及びそれらを含有する有害生物防除剤 |
| JPS57126475A (en) * | 1981-01-28 | 1982-08-06 | Ishihara Sangyo Kaisha Ltd | N-pyridylaniline and pest controller containing the same |
| JPS60123471A (ja) * | 1983-12-07 | 1985-07-02 | Ishihara Sangyo Kaisha Ltd | Ν−（３−クロロ−５−トリフルオロメチル−２−ピリジル）−３−クロロ−２，６−ジニトロ−４−トリフルオロメチルアニリンの製造方法 |
| DE3905238A1 (de) * | 1989-02-21 | 1990-08-23 | Basf Ag | 2-anilino-cyanopyridine und diese enthaltende fungizide |
| NZ600896A (en) * | 2005-11-23 | 2013-12-20 | Makhteshim Chem Works Ltd | Process for preparing pyridinamines and novel polymorphs thereof |
-
2008
- 2008-07-08 JP JP2008178336A patent/JP5390800B2/ja active Active
- 2008-07-22 TW TW097127805A patent/TWI417285B/zh active
- 2008-07-29 SI SI200831323T patent/SI2170829T1/sl unknown
- 2008-07-29 RS RS20140647A patent/RS53735B1/sr unknown
- 2008-07-29 PL PL08792139T patent/PL2170829T3/pl unknown
- 2008-07-29 MX MX2010001191A patent/MX2010001191A/es active IP Right Grant
- 2008-07-29 AU AU2008283242A patent/AU2008283242B2/en active Active
- 2008-07-29 CN CN2008801016245A patent/CN101778824B/zh active Active
- 2008-07-29 GE GEAP200811705A patent/GEP20135742B/en unknown
- 2008-07-29 ES ES08792139.1T patent/ES2503541T3/es active Active
- 2008-07-29 PT PT87921391T patent/PT2170829E/pt unknown
- 2008-07-29 US US12/671,050 patent/US8338612B2/en active Active
- 2008-07-29 BR BRPI0814887A patent/BRPI0814887B1/pt active IP Right Grant
- 2008-07-29 KR KR1020107002325A patent/KR101461259B1/ko active Active
- 2008-07-29 DK DK08792139.1T patent/DK2170829T3/en active
- 2008-07-29 CA CA2694939A patent/CA2694939C/en active Active
- 2008-07-29 RU RU2010107469/04A patent/RU2470919C2/ru active
- 2008-07-29 NZ NZ582589A patent/NZ582589A/en unknown
- 2008-07-29 EP EP08792139.1A patent/EP2170829B1/en active Active
- 2008-07-29 HR HRP20140960AT patent/HRP20140960T1/hr unknown
- 2008-07-29 WO PCT/JP2008/063933 patent/WO2009017241A2/en not_active Ceased
- 2008-08-01 CL CL2008002275A patent/CL2008002275A1/es unknown
- 2008-08-01 AR ARP080103356A patent/AR068801A1/es active IP Right Grant
-
2010
- 2010-01-28 ZA ZA2010/00670A patent/ZA201000670B/en unknown
- 2010-01-31 IL IL203608A patent/IL203608A/en active IP Right Grant
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |