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MX2009009631A - Proceso para la preparacion de esteres metilicos de aminoacido. - Google Patents

Proceso para la preparacion de esteres metilicos de aminoacido.

Info

Publication number
MX2009009631A
MX2009009631A MX2009009631A MX2009009631A MX2009009631A MX 2009009631 A MX2009009631 A MX 2009009631A MX 2009009631 A MX2009009631 A MX 2009009631A MX 2009009631 A MX2009009631 A MX 2009009631A MX 2009009631 A MX2009009631 A MX 2009009631A
Authority
MX
Mexico
Prior art keywords
amino acid
acid methyl
preparation
methyl esters
methanol
Prior art date
Application number
MX2009009631A
Other languages
English (en)
Inventor
Harold Monro Moody
Original Assignee
Dsm Ip Assets Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv
Publication of MX2009009631A publication Critical patent/MX2009009631A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
    • C07C227/18—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions involving amino or carboxyl groups, e.g. hydrolysis of esters or amides, by formation of halides, salts or esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/34—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton containing six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención describe un proceso para la síntesis de un éster metílico de aminoácido que comprende las siguientes etapas: (a) refluir una mezcla de reacción que comprende un aminoácido libre, metanol y un ácido fuerte; (b) concentrar la mezcla; (c) agregar metanol; (d) repetir las etapas a-c una o más veces.
MX2009009631A 2007-03-09 2008-03-10 Proceso para la preparacion de esteres metilicos de aminoacido. MX2009009631A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP07103851 2007-03-09
PCT/EP2008/052814 WO2008110529A1 (en) 2007-03-09 2008-03-10 Process for the preparation of amino acid methyl esters

Publications (1)

Publication Number Publication Date
MX2009009631A true MX2009009631A (es) 2009-09-21

Family

ID=38266673

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2009009631A MX2009009631A (es) 2007-03-09 2008-03-10 Proceso para la preparacion de esteres metilicos de aminoacido.

Country Status (10)

Country Link
US (1) US8039662B2 (es)
EP (1) EP2132166B1 (es)
JP (1) JP5374795B2 (es)
KR (1) KR101470663B1 (es)
CN (1) CN101631764B (es)
BR (1) BRPI0808668B1 (es)
EG (1) EG25838A (es)
ES (1) ES2403033T3 (es)
MX (1) MX2009009631A (es)
WO (1) WO2008110529A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012175587A2 (en) 2011-06-23 2012-12-27 Dsm Sinochem Pharmaceuticals Netherlands B.V. Novel crystalline cefoperazone intermediate
PL2723882T3 (pl) 2011-06-23 2020-01-31 Centrient Pharmaceuticals Netherlands B.V. Sposób wytwarzania 3’-tiopodstawionych cefalosporyn z zastosowaniem acylazy penicyliny
KR101582517B1 (ko) 2015-01-28 2016-01-05 (주)휴빌론 WPS(WIFI positioning system)를 이용한 이동 방향 추정 방법 및 시스템
WO2017021390A1 (en) * 2015-08-04 2017-02-09 Dsm Sinochem Pharmaceuticals Netherlands B.V. Salt of dihydrophenylglycine methyl ester
CN106187795A (zh) * 2016-07-05 2016-12-07 南京红杉生物科技有限公司 一种d‑苯甘氨酸甲酯的合成方法
CN111153821A (zh) * 2019-12-25 2020-05-15 国药集团大同威奇达中抗制药有限公司 D-对羟基苯甘氨酸甲酯的制备方法
CN113387824A (zh) * 2021-07-20 2021-09-14 华北制药股份有限公司 一种高纯度d-二氢苯基甘氨酸甲酯及其制备方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE758860A (fr) * 1969-11-12 1971-05-12 Squibb & Sons Inc Dipeptides
JPS5945667B2 (ja) * 1979-02-08 1984-11-07 東レ株式会社 アミノ酸アミノアルキルエステルの製造方法
US4680403A (en) * 1985-01-17 1987-07-14 Ajinomoto Co., Inc. Process for producing N-protected-α-L-aspartyl-L-phenylalanine methyl ester
JPH01165560A (ja) * 1987-12-23 1989-06-29 Tosoh Corp アミノ酸のエステル化方法
EP0376230B1 (en) * 1988-12-27 1994-11-23 MITSUI TOATSU CHEMICALS, Inc. Preparation and isolation of mineral acid salt of an amino methyl ester
KR930004053A (ko) * 1991-08-09 1993-03-22 김중기 접합 엠보싱 필름의 제조장치
JPH05148199A (ja) * 1991-11-28 1993-06-15 Ajinomoto Co Inc アミノ酸エステルの製造法
JP2009512632A (ja) * 2005-09-29 2009-03-26 ディーエスエム アイピー アセッツ ビー．ブイ． 有機酸のエステル化方法

Also Published As

Publication number Publication date
US20100063312A1 (en) 2010-03-11
EP2132166A1 (en) 2009-12-16
BRPI0808668A2 (pt) 2014-08-26
JP2010520870A (ja) 2010-06-17
CN101631764A (zh) 2010-01-20
US8039662B2 (en) 2011-10-18
BRPI0808668B1 (pt) 2016-12-20
KR20090121311A (ko) 2009-11-25
ES2403033T3 (es) 2013-05-13
EG25838A (en) 2012-09-04
EP2132166B1 (en) 2013-01-16
WO2008110529A1 (en) 2008-09-18
JP5374795B2 (ja) 2013-12-25
CN101631764B (zh) 2013-10-16
KR101470663B1 (ko) 2014-12-08

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