MD97C2 - Способ получения сукралозы - Google Patents
Способ получения сукралозыInfo
- Publication number
- MD97C2 MD97C2 MD94-0113A MD940113A MD97C2 MD 97 C2 MD97 C2 MD 97C2 MD 940113 A MD940113 A MD 940113A MD 97 C2 MD97 C2 MD 97C2
- Authority
- MD
- Moldova
- Prior art keywords
- chlor
- thr
- obtaining
- result
- solution
- Prior art date
Links
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical class [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 4
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 abstract 2
- 102000004190 Enzymes Human genes 0.000 abstract 1
- 108090000790 Enzymes Proteins 0.000 abstract 1
- 102000002464 Galactosidases Human genes 0.000 abstract 1
- 108010093031 Galactosidases Proteins 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 238000011534 incubation Methods 0.000 abstract 1
- 229910000073 phosphorus hydride Inorganic materials 0.000 abstract 1
- 230000002940 repellent Effects 0.000 abstract 1
- 239000005871 repellent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Enzymes And Modification Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
Изобретение относится к биотехнологии.Цель изобретения - упрощение процесса за счет минимизации образования побочных продуктов.Способ предусматривает хлорирование производного сахарозы, замещенного в положении 6, с введением атомов хлора в положение 4,1' и 6' сахарозы и последующее удаление 6-заместителя. В качестве 6-замещенного производного сахарозы используют рафинозу. Удадение 6-заместителя осуществляют путем ферментативного гидролиза 1-15% раствора О-α-Д-6-хлор-6-дезоксигалактопиранозил-(1-6)-α-Д-4-хлор-4-дезоксигалактопиранозил-(1-2)-β-Д-1,6-дихлор-1,6-дидезоксифруктофуранозида в водной системе или в гидрофобном растворителе с использованием - галактозидазы из Mortierella vinacea или Circinella muscat проявляющей степень гидролиза от 1,6 до 4,3 мг сукралозы га 1г сухого клеточного остатка в 1ч при 30-60°С до достижения 50-70%-ной конверсии. Растворитель представляет собой метилизобутилкетон, этилацетат или н-бутанол.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB858525871A GB8525871D0 (en) | 1985-10-21 | 1985-10-21 | Chemical compound |
| SU864028456A SU1635905A3 (ru) | 1985-10-21 | 1986-10-20 | Способ получени сукралозы |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MD97B1 MD97B1 (ro) | 1994-11-30 |
| MD97C2 true MD97C2 (ru) | 1995-03-31 |
Family
ID=26289912
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MD94-0113A MD97C2 (ru) | 1985-10-21 | 1994-03-23 | Способ получения сукралозы |
Country Status (3)
| Country | Link |
|---|---|
| LT (1) | LT2150B (ru) |
| LV (1) | LV5136A3 (ru) |
| MD (1) | MD97C2 (ru) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2079749A (en) * | 1980-07-08 | 1982-01-27 | Tate & Lyle Ltd | Process for the preparation of 4,1',6'-trichloro-4,1',6'- trideoxygalactosucrose |
-
1992
- 1992-12-29 LV LV920526A patent/LV5136A3/xx unknown
-
1993
- 1993-06-22 LT LTRP676A patent/LT2150B/xx not_active IP Right Cessation
-
1994
- 1994-03-23 MD MD94-0113A patent/MD97C2/ru not_active IP Right Cessation
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2079749A (en) * | 1980-07-08 | 1982-01-27 | Tate & Lyle Ltd | Process for the preparation of 4,1',6'-trichloro-4,1',6'- trideoxygalactosucrose |
Also Published As
| Publication number | Publication date |
|---|---|
| MD97B1 (ro) | 1994-11-30 |
| LV5136A3 (lv) | 1993-06-10 |
| LT2150B (lt) | 1993-09-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 1M4A | Expiration of terms |