MD4063C1 - Method for producing nanotubes of titanium dioxide on a titanium substrate - Google Patents
Method for producing nanotubes of titanium dioxide on a titanium substrate Download PDFInfo
- Publication number
- MD4063C1 MD4063C1 MDA20100024A MD20100024A MD4063C1 MD 4063 C1 MD4063 C1 MD 4063C1 MD A20100024 A MDA20100024 A MD A20100024A MD 20100024 A MD20100024 A MD 20100024A MD 4063 C1 MD4063 C1 MD 4063C1
- Authority
- MD
- Moldova
- Prior art keywords
- titanium
- titanium dioxide
- producing
- producing nanotubes
- substrate
- Prior art date
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title abstract 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000002071 nanotube Substances 0.000 title abstract 2
- 229910052719 titanium Inorganic materials 0.000 title abstract 2
- 239000010936 titanium Substances 0.000 title abstract 2
- 239000004408 titanium dioxide Substances 0.000 title abstract 2
- 239000000758 substrate Substances 0.000 title 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 2
- 239000003792 electrolyte Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 1
- 238000005238 degreasing Methods 0.000 abstract 1
- 239000002086 nanomaterial Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
Landscapes
- Catalysts (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
The invention relates to methods for producing nanomaterials, in particular to a method for producing nanotubes of titanium dioxide.The process, according to the invention, includes degreasing of titanium plate and anodic oxidation of its surface in an electrolyte containing hydrofluoric acid, phosphoric acid and ethylene glycol, at the electric current voltage of 50...150 V and the electrolyte temperature of -20...+50°C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDA20100024A MD4063C1 (en) | 2010-02-18 | 2010-02-18 | Method for producing nanotubes of titanium dioxide on a titanium substrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MDA20100024A MD4063C1 (en) | 2010-02-18 | 2010-02-18 | Method for producing nanotubes of titanium dioxide on a titanium substrate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MD4063B1 MD4063B1 (en) | 2010-08-31 |
| MD4063C1 true MD4063C1 (en) | 2011-03-31 |
Family
ID=43569042
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MDA20100024A MD4063C1 (en) | 2010-02-18 | 2010-02-18 | Method for producing nanotubes of titanium dioxide on a titanium substrate |
Country Status (1)
| Country | Link |
|---|---|
| MD (1) | MD4063C1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2732130C1 (en) * | 2019-06-18 | 2020-09-11 | Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method of producing photocatalyst based on nanotubular titanium dioxide |
Citations (23)
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| US6537517B1 (en) * | 1996-09-30 | 2003-03-25 | Chuba Electric Power Co., Ltd. | Crystalline titania having nanotube crystal shape and process for producing the same |
| JP2003238157A (en) * | 2002-02-13 | 2003-08-27 | Toyota Motor Corp | Titania nanotube |
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| JP2004331490A (en) * | 2003-04-15 | 2004-11-25 | Sumitomo Chem Co Ltd | Titania nanotube and method for producing the same |
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| JP2005263616A (en) * | 2004-02-16 | 2005-09-29 | Toray Ind Inc | Method for producing carbon nanotube |
| US20050224360A1 (en) * | 2004-04-02 | 2005-10-13 | The Penn Research Foundation | Titania nanotube arrays for use as sensors and method of producing |
| JP2006089307A (en) * | 2004-09-21 | 2006-04-06 | Inax Corp | Method of producing titania nanotube |
| US20060193766A1 (en) * | 2003-04-15 | 2006-08-31 | Akira Hasegawa | Titania nanotube and method for producing same |
| JP2007054694A (en) * | 2005-08-22 | 2007-03-08 | Tokyo Institute Of Technology | Method for decomposing hardly decomposable organochlorine compound and carbon nanotube composite material |
| CN1974875A (en) * | 2006-11-21 | 2007-06-06 | 北京工业大学 | Prepn process of high length/diameter ratio titania nanotube array film |
| KR100810122B1 (en) * | 2007-03-07 | 2008-03-06 | 한국에너지기술연구원 | Contact Combustion Gas Sensor with Titanium Oxide Nanotubes Dispersed with Palladium and Platinum |
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| CN101234781A (en) * | 2008-02-29 | 2008-08-06 | 福州大学 | Preparation method of high-purity brookite titanium dioxide nanotube |
| US20080241123A1 (en) * | 2005-10-14 | 2008-10-02 | Dewan Fazlul Hoque Chowdhury | Amphiphilic Nanotubes And Micelles Comprising Same For Use In The Delivery of Biologically Active Agents |
| MD3535G2 (en) * | 2007-03-21 | 2008-10-31 | Государственный Университет Молд0 | Process for nanodispersed titanium dioxide obtaining |
| CN101302036A (en) * | 2008-07-03 | 2008-11-12 | 南开大学 | A kind of preparation method of doped titanium dioxide nanotube |
| JP2009035463A (en) * | 2007-08-03 | 2009-02-19 | National Institute Of Advanced Industrial & Technology | Carbon nanosheet / titanate nanotube composite, carbon nanosheet / titania nanorod composite, production method thereof and use thereof |
| CN101531396A (en) * | 2009-04-22 | 2009-09-16 | 湖南大学 | TiO2 nanotube with molecular imprinting functionalization |
| MD3977B1 (en) * | 2008-11-11 | 2009-11-30 | Universitatea De Stat Din Moldova | Process for nanodispersed titanium dioxide obtaining |
| US20100006134A1 (en) * | 2004-03-19 | 2010-01-14 | Nippon Oil Corporation | Nanotube-shaped titania and process for producing the same |
| US20100024879A1 (en) * | 2007-02-21 | 2010-02-04 | Northeastern University | Titania nanotubes prepared by anodization in chloride-containing electrolytes |
| EP2191040A2 (en) * | 2007-07-26 | 2010-06-02 | The Penn State Research Foundation | Highly-ordered titania nanotube arrays |
-
2010
- 2010-02-18 MD MDA20100024A patent/MD4063C1/en not_active IP Right Cessation
Patent Citations (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6537517B1 (en) * | 1996-09-30 | 2003-03-25 | Chuba Electric Power Co., Ltd. | Crystalline titania having nanotube crystal shape and process for producing the same |
| JP2003238157A (en) * | 2002-02-13 | 2003-08-27 | Toyota Motor Corp | Titania nanotube |
| KR20030082431A (en) * | 2002-04-15 | 2003-10-22 | 주식회사 엘지화학 | Electropolymerization method for preparing nano-tube type conducting polymer using porous template, method for preparing electrochromic device, and electrochromic device prepared therefrom |
| US20060193766A1 (en) * | 2003-04-15 | 2006-08-31 | Akira Hasegawa | Titania nanotube and method for producing same |
| JP2004331490A (en) * | 2003-04-15 | 2004-11-25 | Sumitomo Chem Co Ltd | Titania nanotube and method for producing the same |
| JP2005263616A (en) * | 2004-02-16 | 2005-09-29 | Toray Ind Inc | Method for producing carbon nanotube |
| US20100006134A1 (en) * | 2004-03-19 | 2010-01-14 | Nippon Oil Corporation | Nanotube-shaped titania and process for producing the same |
| US20050224360A1 (en) * | 2004-04-02 | 2005-10-13 | The Penn Research Foundation | Titania nanotube arrays for use as sensors and method of producing |
| US7011737B2 (en) * | 2004-04-02 | 2006-03-14 | The Penn State Research Foundation | Titania nanotube arrays for use as sensors and method of producing |
| MD2585G2 (en) * | 2004-06-01 | 2005-05-31 | Ион ТИГИНЯНУ | Process for semiconductor nanostructures obtaining |
| JP2006089307A (en) * | 2004-09-21 | 2006-04-06 | Inax Corp | Method of producing titania nanotube |
| JP2007054694A (en) * | 2005-08-22 | 2007-03-08 | Tokyo Institute Of Technology | Method for decomposing hardly decomposable organochlorine compound and carbon nanotube composite material |
| US20080241123A1 (en) * | 2005-10-14 | 2008-10-02 | Dewan Fazlul Hoque Chowdhury | Amphiphilic Nanotubes And Micelles Comprising Same For Use In The Delivery of Biologically Active Agents |
| CN1974875A (en) * | 2006-11-21 | 2007-06-06 | 北京工业大学 | Prepn process of high length/diameter ratio titania nanotube array film |
| US20100024879A1 (en) * | 2007-02-21 | 2010-02-04 | Northeastern University | Titania nanotubes prepared by anodization in chloride-containing electrolytes |
| KR100810122B1 (en) * | 2007-03-07 | 2008-03-06 | 한국에너지기술연구원 | Contact Combustion Gas Sensor with Titanium Oxide Nanotubes Dispersed with Palladium and Platinum |
| MD3535G2 (en) * | 2007-03-21 | 2008-10-31 | Государственный Университет Молд0 | Process for nanodispersed titanium dioxide obtaining |
| EP2191040A2 (en) * | 2007-07-26 | 2010-06-02 | The Penn State Research Foundation | Highly-ordered titania nanotube arrays |
| JP2009035463A (en) * | 2007-08-03 | 2009-02-19 | National Institute Of Advanced Industrial & Technology | Carbon nanosheet / titanate nanotube composite, carbon nanosheet / titania nanorod composite, production method thereof and use thereof |
| CN101187043A (en) * | 2007-09-17 | 2008-05-28 | 西北有色金属研究院 | Preparation method of ultralong titania nanotube arrays with photocatalytic properties |
| CN101234781A (en) * | 2008-02-29 | 2008-08-06 | 福州大学 | Preparation method of high-purity brookite titanium dioxide nanotube |
| CN101302036A (en) * | 2008-07-03 | 2008-11-12 | 南开大学 | A kind of preparation method of doped titanium dioxide nanotube |
| MD3977B1 (en) * | 2008-11-11 | 2009-11-30 | Universitatea De Stat Din Moldova | Process for nanodispersed titanium dioxide obtaining |
| CN101531396A (en) * | 2009-04-22 | 2009-09-16 | 湖南大学 | TiO2 nanotube with molecular imprinting functionalization |
Non-Patent Citations (6)
| Title |
|---|
| Albu S.P., Ghicov A., Macak J.M., Hahn R., Schmuki P. Self-organized, free-standing TiO2 nanotube membrane for flow-through photocatalytic * |
| applications. Nano Letters, 2007, V. 5(7), p. 1286-1289. * |
| Mor G.K., Varghese O.K., Paulose M., Shankar K., Grimes C.A A review on highly ordered vertically oriented TiO2 nanotube arrays: Fabrication, material * |
| Mor G.K., Varghese O.K., Paulose M., Shankar K., Grimes C.A. A review on highly ordered vertically oriented TiO2 nanotube arrays: Fabrication, material properties, and solar energy applications. Solar Energy Materials & Solar cell, 2006, V. 90, p. 2011-2075. * |
| properties, and solar energy applications.Solar Energy Materials & Solar cell, 2006, V. 90, p. 2011-2075. * |
| S.P., Ghicov A., Macak J.M., Hahn R., Schmuki P. Self-organized, free-standing TiO2 nanotube membrane for flow-through photocatalytic applications. Nano Letters, 2007, V. 5(7), p. 1286-1289. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2732130C1 (en) * | 2019-06-18 | 2020-09-11 | Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина" | Method of producing photocatalyst based on nanotubular titanium dioxide |
Also Published As
| Publication number | Publication date |
|---|---|
| MD4063B1 (en) | 2010-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG4A | Patent for invention issued | ||
| KA4A | Patent for invention lapsed due to non-payment of fees (with right of restoration) | ||
| MM4A | Patent for invention definitely lapsed due to non-payment of fees |