MA48430B1 - Procédé et dispositif de préparation de solutions de sel de leucoindigo exemptes d'aniline - Google Patents
Procédé et dispositif de préparation de solutions de sel de leucoindigo exemptes d'anilineInfo
- Publication number
- MA48430B1 MA48430B1 MA48430A MA48430A MA48430B1 MA 48430 B1 MA48430 B1 MA 48430B1 MA 48430 A MA48430 A MA 48430A MA 48430 A MA48430 A MA 48430A MA 48430 B1 MA48430 B1 MA 48430B1
- Authority
- MA
- Morocco
- Prior art keywords
- aniline
- free
- leucoindigo
- salt solutions
- methylaniline
- Prior art date
Links
- VIFKLIUAPGUEBV-UHFFFAOYSA-N 2-(3-hydroxy-1h-indol-2-yl)-1h-indol-3-ol Chemical class N1C2=CC=CC=C2C(O)=C1C1=C(O)C2=CC=CC=C2N1 VIFKLIUAPGUEBV-UHFFFAOYSA-N 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- 239000012266 salt solution Substances 0.000 title 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 12
- AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methylaniline Chemical compound CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 abstract 6
- 239000007864 aqueous solution Substances 0.000 abstract 3
- 239000007788 liquid Substances 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- -1 alkali metal salt Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0083—Solutions of dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0077—Preparations with possibly reduced vat, sulfur or indigo dyes
- C09B67/0078—Preparations of vat, sulfur or indigo dyes in liquid form
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/02—Bis-indole indigos
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/228—Indigo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Indole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Peptides Or Proteins (AREA)
Abstract
L'invention concerne un procédé de préparation d'une solution aqueuse de leucoindigo exempte d'aniline ou exempte d'aniline et exempte de n-méthylaniline à partir d'une solution aqueuse de leucoindigo comprenant de l'aniline ou de l'aniline et de la n-méthylaniline, la concentration en aniline ou en aniline et en n-méthylaniline étant déterminée selon la norme iso 14362-1:2017(e), ledit leucoindigo se présentant sous la forme d'un sel de métal alcalin, le procédé comprenant au moins les étapes (a) à (c) consistant à : (a) utiliser un flux de liquide comprenant ladite solution aqueuse de leucoindigo comprenant ladite ou lesdites amines ; (b) utiliser un flux de purification ; (c) mettre en contact ledit flux de liquide avec ledit flux de purification.
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17185976.2A EP3441430B1 (fr) | 2017-08-11 | 2017-08-11 | Solution de sel de leucoindigo à très faible teneur d'aniline et son procédé de fabrication |
| EP17185980.4A EP3441431B1 (fr) | 2017-08-11 | 2017-08-11 | Procédés de fabrication de solutions de sel leucoindigo avec très faible contenu d'aniline |
| EP17185971.3A EP3441429B1 (fr) | 2017-08-11 | 2017-08-11 | Solutions aqueuses concentrées et purifiées de sel de leucoindigo |
| EP18173343.7A EP3569660B1 (fr) | 2018-05-18 | 2018-05-18 | Procédé pour fabriquer des solutions de sel de leucoindigo sans aniline |
| PCT/EP2018/071805 WO2019030397A1 (fr) | 2017-08-11 | 2018-08-10 | Procédé et dispositif de préparation de solutions de sel de leucoindigo exemptes d'aniline |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MA48430A1 MA48430A1 (fr) | 2020-04-30 |
| MA48430B1 true MA48430B1 (fr) | 2020-11-30 |
Family
ID=63108593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MA48430A MA48430B1 (fr) | 2017-08-11 | 2018-08-10 | Procédé et dispositif de préparation de solutions de sel de leucoindigo exemptes d'aniline |
Country Status (15)
| Country | Link |
|---|---|
| US (4) | US11299633B2 (fr) |
| EP (5) | EP3665229A1 (fr) |
| JP (6) | JP7250762B2 (fr) |
| KR (6) | KR102687719B1 (fr) |
| CN (5) | CN111065690B (fr) |
| AR (2) | AR126783A2 (fr) |
| BR (4) | BR112019018497B1 (fr) |
| CO (3) | CO2020001381A2 (fr) |
| MA (1) | MA48430B1 (fr) |
| MX (4) | MX2020001519A (fr) |
| PE (5) | PE20201187A1 (fr) |
| SG (4) | SG11202001153RA (fr) |
| TN (4) | TN2020000011A1 (fr) |
| TW (4) | TWI755558B (fr) |
| WO (4) | WO2019030396A1 (fr) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PE20201187A1 (es) | 2017-08-11 | 2020-11-06 | Archroma Ip Gmbh | Solucion de sal de leucoindigo con muy bajo contenido de anilina y metodo para realizar la misma |
| CN110016816A (zh) * | 2019-03-13 | 2019-07-16 | 广东前进牛仔布有限公司 | 一种靛蓝染色方法 |
| BR102019025172A2 (pt) | 2019-11-28 | 2021-06-08 | Bann Química Ltda. | processo de purificação de soluções de sal de leucoíndigo e uso de um gás inerte |
| JP2021094344A (ja) * | 2019-12-19 | 2021-06-24 | サミー株式会社 | ぱちんこ遊技機 |
| JP2021094346A (ja) * | 2019-12-19 | 2021-06-24 | サミー株式会社 | ぱちんこ遊技機 |
| CN118925746B (zh) * | 2024-07-22 | 2025-06-27 | 重庆市化工研究院有限公司 | 一种用于生产还原靛蓝的雷尼镍催化剂及还原靛蓝的生产方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2130878A (en) * | 1933-04-10 | 1938-09-20 | Ici Ltd | Leucoindigo |
| US4992143A (en) * | 1989-06-09 | 1991-02-12 | Mobay Corporation | Continuous process for the separation of a partially water soluble component from a slurry |
| US5116996A (en) * | 1991-07-17 | 1992-05-26 | Basf Aktiengesellschaft | Purification of indigo |
| US6169218B1 (en) | 1992-02-10 | 2001-01-02 | Catalytic Distillation Technologies | Selective hydrogenation of highly unsaturated compounds in hydrocarbon streams |
| DE4220804A1 (de) * | 1992-06-25 | 1994-01-05 | Basf Ag | Verfahren zur Reinigung von Indigo |
| TW251325B (fr) | 1993-03-30 | 1995-07-11 | Basf Ag | |
| DE4327221A1 (de) * | 1993-08-13 | 1995-02-16 | Basf Ag | Leukoindigo-Präparation in Granulatform |
| DE4336032A1 (de) * | 1993-10-22 | 1995-04-27 | Basf Ag | Verfahren zur Reinigung von Indigo |
| DE19502968A1 (de) * | 1995-01-31 | 1996-08-01 | Basf Ag | Leukoküpenfarbstoff-Präparationen in Granulatform |
| DE19624208A1 (de) * | 1996-06-18 | 1998-01-02 | Basf Ag | Leukoküpenfarbstoff-Präparationen in Granulatform |
| JPH10111633A (ja) * | 1996-10-04 | 1998-04-28 | Denso Corp | ホログラム感光剤,ホログラム感光材料及びホログラム,並びにこれらの製造方法 |
| DE19831291A1 (de) | 1998-07-13 | 2000-01-20 | Basf Ag | Konzentrierte Lekoindigolösungen |
| DE19919746A1 (de) * | 1999-04-29 | 2000-11-02 | Basf Ag | Verfahren zur Herstellung von wäßrig-alkalischen Lösungen reduzierter indigoider Farbstoffe |
| WO2004024826A2 (fr) | 2002-08-31 | 2004-03-25 | Dystar Textilfarben Gmbh & Co. Deutschland Kg | Procede pour produire de l'indigo de tres grande purete |
| JP4941891B2 (ja) | 2006-11-13 | 2012-05-30 | 株式会社Ihi | フィルム冷却構造 |
| JP2009197353A (ja) * | 2008-02-20 | 2009-09-03 | Asahi Breweries Ltd | インヂゴの染色増強剤および増強方法 |
| PE20201187A1 (es) * | 2017-08-11 | 2020-11-06 | Archroma Ip Gmbh | Solucion de sal de leucoindigo con muy bajo contenido de anilina y metodo para realizar la misma |
| ES2883323T3 (es) * | 2017-08-11 | 2021-12-07 | Archroma Ip Gmbh | Métodos de fabricación de soluciones de sal de leucoíndigo con contenido de anilina muy bajo |
| PT3441429T (pt) * | 2017-08-11 | 2021-06-28 | Archroma Ip Gmbh | Soluções de sal de leucoindigo aquoso purificado concentrado |
| ES2841500T3 (es) * | 2017-08-11 | 2021-07-08 | Archroma Ip Gmbh | Solución de sal de leucoíndigo con muy bajo contenido de anilina y método de preparar la misma |
| ES2900511T3 (es) * | 2018-05-18 | 2022-03-17 | Archroma Ip Gmbh | Método para preparar soluciones de sal de leucoíndigo sin anilina |
-
2018
- 2018-08-10 PE PE2020000206A patent/PE20201187A1/es unknown
- 2018-08-10 TN TNP/2020/000011A patent/TN2020000011A1/en unknown
- 2018-08-10 TW TW107127916A patent/TWI755558B/zh active
- 2018-08-10 JP JP2020507661A patent/JP7250762B2/ja active Active
- 2018-08-10 KR KR1020207007081A patent/KR102687719B1/ko active Active
- 2018-08-10 EP EP18750226.5A patent/EP3665229A1/fr not_active Withdrawn
- 2018-08-10 TW TW107127918A patent/TWI763904B/zh active
- 2018-08-10 TN TNP/2020/000012A patent/TN2020000012A1/en unknown
- 2018-08-10 BR BR112019018497-0A patent/BR112019018497B1/pt active IP Right Grant
- 2018-08-10 PE PE2020000209A patent/PE20200787A1/es unknown
- 2018-08-10 KR KR1020207007084A patent/KR102636594B1/ko active Active
- 2018-08-10 EP EP18750227.3A patent/EP3665230A1/fr not_active Withdrawn
- 2018-08-10 MA MA48430A patent/MA48430B1/fr unknown
- 2018-08-10 KR KR1020207007074A patent/KR102636591B1/ko active Active
- 2018-08-10 CN CN201880059273.XA patent/CN111065690B/zh active Active
- 2018-08-10 TW TW107127915A patent/TWI763903B/zh active
- 2018-08-10 CN CN201880059267.4A patent/CN111108156A/zh active Pending
- 2018-08-10 TW TW107127917A patent/TWI760544B/zh active
- 2018-08-10 TN TNP/2020/000014A patent/TN2020000014A1/en unknown
- 2018-08-10 KR KR1020207007071A patent/KR20200040278A/ko not_active Ceased
- 2018-08-10 WO PCT/EP2018/071800 patent/WO2019030396A1/fr not_active Ceased
- 2018-08-10 JP JP2020507600A patent/JP7011042B2/ja active Active
- 2018-08-10 CN CN201880059304.1A patent/CN111094460A/zh active Pending
- 2018-08-10 WO PCT/EP2018/071791 patent/WO2019030391A1/fr not_active Ceased
- 2018-08-10 JP JP2020507660A patent/JP7245227B2/ja active Active
- 2018-08-10 WO PCT/EP2018/071805 patent/WO2019030397A1/fr not_active Ceased
- 2018-08-10 MX MX2020001519A patent/MX2020001519A/es unknown
- 2018-08-10 US US16/637,874 patent/US11299633B2/en active Active
- 2018-08-10 JP JP2020507643A patent/JP7295844B2/ja active Active
- 2018-08-10 BR BR112019018498A patent/BR112019018498A2/pt not_active Application Discontinuation
- 2018-08-10 MX MX2020001517A patent/MX2020001517A/es unknown
- 2018-08-10 EP EP18750225.7A patent/EP3665228A1/fr not_active Withdrawn
- 2018-08-10 TN TNP/2020/000013A patent/TN2020000013A1/en unknown
- 2018-08-10 PE PE2025000454A patent/PE20250954A1/es unknown
- 2018-08-10 SG SG11202001153RA patent/SG11202001153RA/en unknown
- 2018-08-10 CN CN202211229474.4A patent/CN115627081B/zh active Active
- 2018-08-10 MX MX2020001518A patent/MX2020001518A/es unknown
- 2018-08-10 US US16/637,889 patent/US20200216674A1/en not_active Abandoned
- 2018-08-10 PE PE2020000210A patent/PE20201188A1/es unknown
- 2018-08-10 WO PCT/EP2018/071783 patent/WO2019030389A1/fr not_active Ceased
- 2018-08-10 CN CN201880059274.4A patent/CN111133057B/zh active Active
- 2018-08-10 US US16/637,862 patent/US11384245B2/en active Active
- 2018-08-10 KR KR1020217023586A patent/KR20210114958A/ko not_active Ceased
- 2018-08-10 BR BR112019018494-5A patent/BR112019018494B1/pt active IP Right Grant
- 2018-08-10 MX MX2020001516A patent/MX2020001516A/es unknown
- 2018-08-10 SG SG11202001155UA patent/SG11202001155UA/en unknown
- 2018-08-10 EP EP25175754.8A patent/EP4575077A3/fr active Pending
- 2018-08-10 PE PE2020000207A patent/PE20200786A1/es unknown
- 2018-08-10 EP EP18750223.2A patent/EP3665227A1/fr not_active Withdrawn
- 2018-08-10 KR KR1020227042817A patent/KR102706455B1/ko active Active
- 2018-08-10 SG SG11202001152YA patent/SG11202001152YA/en unknown
- 2018-08-10 BR BR112019018490-2A patent/BR112019018490B1/pt active IP Right Grant
- 2018-08-10 SG SG11202001151PA patent/SG11202001151PA/en unknown
- 2018-08-10 US US16/637,886 patent/US20200172734A1/en active Pending
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2020
- 2020-02-07 CO CONC2020/0001381A patent/CO2020001381A2/es unknown
- 2020-02-07 CO CONC2020/0001376A patent/CO2020001376A2/es unknown
- 2020-02-07 CO CONC2020/0001377A patent/CO2020001377A2/es unknown
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2022
- 2022-08-12 AR ARP220102183A patent/AR126783A2/es unknown
- 2022-10-14 AR ARP220102811A patent/AR127380A2/es unknown
- 2022-11-21 JP JP2022185474A patent/JP7527337B2/ja active Active
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2023
- 2023-02-28 JP JP2023029566A patent/JP7610636B2/ja active Active
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