Steele et al., 1993 - Google Patents
Monitoring reaction exotherms in pilot scale batch reactorsSteele et al., 1993
- Document ID
- 2820578173851491039
- Author
- Steele C
- Nolan P
- Lowe J
- Hirst A
- Starkie A
- Publication year
- Publication venue
- Journal of loss prevention in the process industries
External Links
Snippet
A method is described in which bench scale heat flow calorimetry data can be used to monitor a chemical reaction at the pilot scale level. A reaction involving dimsyl sodium formation and ester coupling is used as an example to illustrate the methodology. The …
- 238000006243 chemical reaction 0 title abstract description 112
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4846—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample
- G01N25/4866—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample by using a differential method
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