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RU2012144084A - METHOD FOR PRODUCING DI- {4 - [(TETRAHYDRO-4H-1,4-OXAZAZIN-4-IL) -METHYL SULFANIL] -PHENYL} ETHER OF AN OXALOXIDE WATER-SOLUBLE MEANS WITH FUNGICIDAL ACTIVITY - Google Patents

METHOD FOR PRODUCING DI- {4 - [(TETRAHYDRO-4H-1,4-OXAZAZIN-4-IL) -METHYL SULFANIL] -PHENYL} ETHER OF AN OXALOXIDE WATER-SOLUBLE MEANS WITH FUNGICIDAL ACTIVITY Download PDF

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RU2012144084A
RU2012144084A RU2012144084/04A RU2012144084A RU2012144084A RU 2012144084 A RU2012144084 A RU 2012144084A RU 2012144084/04 A RU2012144084/04 A RU 2012144084/04A RU 2012144084 A RU2012144084 A RU 2012144084A RU 2012144084 A RU2012144084 A RU 2012144084A
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tetrahydro
phenyl
ether
water
fungicidal activity
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RU2012144084/04A
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RU2541535C2 (en
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Усеин Меметович Джемилев
Асхат Габдрахманович Ибрагимов
Регина Радиевна Хайруллина
Байрас Фаритович Акманов
Альфия Равзатовна Гениятова
Диана Валиевна Хасанова
Альберт Магсумович Ямалеев
Регина Альбертовна Хайруллина
Анна Александровна Ямалеева
Расиль Расихович Урманов
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Федеральное государственное бюджетное учреждение науки Институт нефтехимии и катализа Российской академии наук
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Abstract

1. Способ получения ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фенилового}эфира щавелевокислого формулы общей формулы (1):отличающийся тем, что ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фениловый}эфир подвергают взаимодействию с эквимольным количеством щавелевой кислоты (СООН), перемешивают в течение 15 мин при комнатной (~20°С) температуре и атмосферном давлении.2. Ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фениловый}щавелевокислый - водорастворимое средство с фунгицидной активностью.1. The method of obtaining di- {4 - [(tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} ester of oxalic acid formula of the general formula (1): characterized in that di- {4- [ (tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} ether is reacted with an equimolar amount of oxalic acid (COOH), stirred for 15 min at room (~ 20 ° C) temperature and atmospheric pressure .2. Di- {4 - [(tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} oxalate is a water-soluble agent with fungicidal activity.

Claims (2)

1. Способ получения ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фенилового}эфира щавелевокислого формулы общей формулы (1):1. The method of obtaining di- {4 - [(tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} ester of oxalic acid formula of the general formula (1):
Figure 00000001
Figure 00000001
 отличающийся тем, что ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фениловый}эфир подвергают взаимодействию с эквимольным количеством щавелевой кислоты (СООН)2, перемешивают в течение 15 мин при комнатной (~20°С) температуре и атмосферном давлении.characterized in that the di- {4 - [(tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} ether is reacted with an equimolar amount of oxalic acid (COOH) 2 , stirred for 15 minutes at room (~ 20 ° C) temperature and atmospheric pressure. 2. Ди-{4-[(тетрагидро-4H-1,4-оксазин-4-ил)-метилсульфанил]-фениловый}щавелевокислый - водорастворимое средство с фунгицидной активностью. 2. Di- {4 - [(tetrahydro-4H-1,4-oxazin-4-yl) methylsulfanyl] phenyl} oxalate - a water-soluble agent with fungicidal activity.
RU2012144084/04A 2012-10-16 2012-10-16 Method of obtaining di-{ 4-[(tetrahydro -4h-1,4-oxazin-4-yl)-methylsulphanyl]-phenyl} ether oxalate - water-soluble substance with fungicidal activity RU2541535C2 (en)

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RU2012144084/04A RU2541535C2 (en) 2012-10-16 2012-10-16 Method of obtaining di-{ 4-[(tetrahydro -4h-1,4-oxazin-4-yl)-methylsulphanyl]-phenyl} ether oxalate - water-soluble substance with fungicidal activity

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