DK127989D0 - PROCEDURE FOR SYNTHESIS OF ARYLSULPHONYLALKYLAMIDS - Google Patents
PROCEDURE FOR SYNTHESIS OF ARYLSULPHONYLALKYLAMIDSInfo
- Publication number
- DK127989D0 DK127989D0 DK127989A DK127989A DK127989D0 DK 127989 D0 DK127989 D0 DK 127989D0 DK 127989 A DK127989 A DK 127989A DK 127989 A DK127989 A DK 127989A DK 127989 D0 DK127989 D0 DK 127989D0
- Authority
- DK
- Denmark
- Prior art keywords
- synthesis
- excess
- arylsulphonylalkylamids
- procedure
- arylsulphonyl halide
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- IPRJXAGUEGOFGG-UHFFFAOYSA-N N-Butylbenzenesulfonamide Natural products CCCCNS(=O)(=O)C1=CC=CC=C1 IPRJXAGUEGOFGG-UHFFFAOYSA-N 0.000 abstract 2
- -1 arylsulphonyl halide Chemical class 0.000 abstract 2
- 239000004952 Polyamide Substances 0.000 abstract 1
- 150000003973 alkyl amines Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 229920002647 polyamide Polymers 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C311/15—Sulfonamides having sulfur atoms of sulfonamide groups bound to carbon atoms of six-membered aromatic rings
- C07C311/16—Sulfonamides having sulfur atoms of sulfonamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the sulfonamide groups bound to hydrogen atoms or to an acyclic carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/38—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reaction of ammonia or amines with sulfonic acids, or with esters, anhydrides, or halides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Steroid Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Polyamides (AREA)
Abstract
Process for the synthesis of arylsulphonylalkylamides in which an arylsulphonyl halide is placed in contact with an excess of alkylamine and an aqueous solution of alkaline agent in excess in relation to the arylsulphonyl halide and then the water and excess amine are removed from the organic phase; the arylsulphonylalkylamide is then isolated. This process is particularly suited for N-n-butylbenzenesulphonamide which is obtained in a thermally stable quality and which can be advantageously employed as a plasticiser for polyamides.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8803447A FR2628739B1 (en) | 1988-03-17 | 1988-03-17 | PROCESS FOR THE SYNTHESIS OF ARYLSULFONYLALKYLAMIDE |
| FR8803447 | 1988-03-17 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DK127989D0 true DK127989D0 (en) | 1989-03-16 |
| DK127989A DK127989A (en) | 1989-09-18 |
| DK175638B1 DK175638B1 (en) | 2005-01-03 |
Family
ID=9364346
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK198901279A DK175638B1 (en) | 1988-03-17 | 1989-03-16 | Process for the synthesis of arylsulfonylalkylamides |
Country Status (14)
| Country | Link |
|---|---|
| EP (1) | EP0333557B1 (en) |
| JP (1) | JPH024766A (en) |
| KR (1) | KR940010765B1 (en) |
| CN (1) | CN1020600C (en) |
| AT (1) | ATE101129T1 (en) |
| CA (1) | CA1307295C (en) |
| DE (1) | DE68912797T2 (en) |
| DK (1) | DK175638B1 (en) |
| ES (1) | ES2062055T3 (en) |
| FI (1) | FI90763C (en) |
| FR (1) | FR2628739B1 (en) |
| IE (1) | IE63494B1 (en) |
| NO (1) | NO170412C (en) |
| PT (1) | PT90025B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1993005014A1 (en) * | 1991-09-05 | 1993-03-18 | Pharno-Wedropharm Gmbh | Aromatic sulfonamide derivatives, their use as enzyme inhibitors and pharmaceutical compositions containing them |
| TW219358B (en) * | 1991-12-20 | 1994-01-21 | Hokuriku Pharmaceutical | |
| GB9625781D0 (en) * | 1996-12-11 | 1997-01-29 | Zeneca Ltd | Chemical process |
| JP5076682B2 (en) * | 2006-07-26 | 2012-11-21 | セントラル硝子株式会社 | Process for producing N- (bicyclo [2,2,1] hept-5-en-2-ylmethyl) -1,1,1-trifluoromethanesulfonamide |
| CN109369473A (en) * | 2018-09-19 | 2019-02-22 | 南通沃兰化工有限公司 | A kind of synthetic method of N-butylbenzenesulfonamide |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2833650A1 (en) * | 1978-08-01 | 1980-02-21 | Basf Ag | METHOD FOR PRODUCING THERMOSTABLE ARYLSULFONYLALKYLAMIDES |
| DE2941593A1 (en) * | 1979-10-13 | 1981-04-23 | Bayer Ag, 5090 Leverkusen | METHOD FOR PRODUCING SULPHONAMIDES |
-
1988
- 1988-03-17 FR FR8803447A patent/FR2628739B1/en not_active Expired - Lifetime
-
1989
- 1989-02-20 CA CA000591539A patent/CA1307295C/en not_active Expired - Lifetime
- 1989-03-01 NO NO890864A patent/NO170412C/en not_active IP Right Cessation
- 1989-03-07 ES ES89400638T patent/ES2062055T3/en not_active Expired - Lifetime
- 1989-03-07 AT AT89400638T patent/ATE101129T1/en not_active IP Right Cessation
- 1989-03-07 DE DE68912797T patent/DE68912797T2/en not_active Expired - Lifetime
- 1989-03-07 EP EP89400638A patent/EP0333557B1/en not_active Expired - Lifetime
- 1989-03-15 JP JP1063399A patent/JPH024766A/en active Granted
- 1989-03-16 DK DK198901279A patent/DK175638B1/en not_active IP Right Cessation
- 1989-03-16 FI FI891256A patent/FI90763C/en not_active IP Right Cessation
- 1989-03-16 IE IE85889A patent/IE63494B1/en not_active IP Right Cessation
- 1989-03-16 PT PT90025A patent/PT90025B/en not_active IP Right Cessation
- 1989-03-17 KR KR1019890003358A patent/KR940010765B1/en not_active Expired - Lifetime
- 1989-03-17 CN CN89101437A patent/CN1020600C/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0333557A3 (en) | 1990-10-17 |
| CN1020600C (en) | 1993-05-12 |
| FI891256A0 (en) | 1989-03-16 |
| IE63494B1 (en) | 1995-05-03 |
| DK127989A (en) | 1989-09-18 |
| PT90025B (en) | 1994-05-31 |
| DE68912797T2 (en) | 1994-06-01 |
| NO170412C (en) | 1992-10-14 |
| FI90763B (en) | 1993-12-15 |
| ATE101129T1 (en) | 1994-02-15 |
| CN1037894A (en) | 1989-12-13 |
| JPH0465063B2 (en) | 1992-10-16 |
| FI90763C (en) | 1994-03-25 |
| FR2628739B1 (en) | 1990-09-07 |
| DK175638B1 (en) | 2005-01-03 |
| NO890864D0 (en) | 1989-03-01 |
| IE890858L (en) | 1989-09-17 |
| KR890014464A (en) | 1989-10-23 |
| KR940010765B1 (en) | 1994-11-11 |
| EP0333557A2 (en) | 1989-09-20 |
| JPH024766A (en) | 1990-01-09 |
| NO890864L (en) | 1989-09-18 |
| ES2062055T3 (en) | 1994-12-16 |
| PT90025A (en) | 1989-11-10 |
| DE68912797D1 (en) | 1994-03-17 |
| FR2628739A1 (en) | 1989-09-22 |
| FI891256L (en) | 1989-09-18 |
| EP0333557B1 (en) | 1994-02-02 |
| CA1307295C (en) | 1992-09-08 |
| NO170412B (en) | 1992-07-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUP | Patent expired |