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DE1051815B - Process for granulating powders - Google Patents

Process for granulating powders

Info

Publication number
DE1051815B
DE1051815B DEF21586A DEF0021586A DE1051815B DE 1051815 B DE1051815 B DE 1051815B DE F21586 A DEF21586 A DE F21586A DE F0021586 A DEF0021586 A DE F0021586A DE 1051815 B DE1051815 B DE 1051815B
Authority
DE
Germany
Prior art keywords
granules
granulating powders
granulating
rolling process
powders
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEF21586A
Other languages
German (de)
Inventor
Dipl-Ing Rudolf Erdmenger
Dr Hans Rumpf
Dr Richard Schlee
Dr Wolfgang Stroh
Dipl-Ing Julius Wehn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DEF20087A external-priority patent/DE1041472B/en
Application filed by Bayer AG filed Critical Bayer AG
Priority to DEF21586A priority Critical patent/DE1051815B/en
Publication of DE1051815B publication Critical patent/DE1051815B/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/18Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using a vibrating apparatus

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Glanulating (AREA)
  • Medicinal Preparation (AREA)

Description

DEUTSCHESGERMAN

Die Hauptpatentammeidung F 20087 IVa/12g betrifft ein Verfahren zur Granulierung feiner Pulver zu Granulaten gewünschter Korngröße ohne Zusatz von Bindemitteln, bei dem nach einem vorzugsweise klassierenden Anigranulierverfahren Keimgranulate mit definiertem Korngrößenbereich erzeugt werden und diese in einem anschließenden, eine Aufbaugranulation begünstigenden Prozeß mit Relativbewegung der Teilchen zu größeren und/oder dichteren Fertiggranulaten umgewandelt werden. Nach diesem Verfahren können Granulate mit hervorragenden Fließeigenschaften hergestellt werden, die sich beispielsweise in begasten Rinnen flüssigkeitsähnlich fortbewegen. Solche Granulate können je nach Dauer und Art der Nachbehandlung im Rollprozeß eine mehr oder minder große Druckfestigkeit erhalten.The main patent F 20087 IVa / 12g relates to a process for granulating fine powders to granules of the desired grain size without the addition of binders, in which case one is preferred seed granulates with a defined grain size range can be produced and this in a subsequent process with relative movement that promotes build-up granulation the particles are converted into larger and / or denser finished granules. After this Process, granules with excellent flow properties can be produced, for example move in a liquid-like manner in fumigated channels. Such granules can vary depending on the duration and type of aftertreatment in the rolling process obtain a more or less high compressive strength.

Es hat sich nun gezeigt, daß man eine Erhöhung der Druckfestigkeit der Granulate erreichen kann, wenn erfindungsgemäß das staub- oder pulverförmige Gut in vorverdichtetem Zustand der Keimgranulierang zugeführt wird.· Der Vorrichtung zur Herstellung der Keimgranulate werden Verdichtungsvorrichtungen für das Pulver, z. B. elastisch gelagerte Preßwalzen, zwischen denen das Gut auf luftdurchlässigen Transportbändern geführt wind, vorgeschaltet. So vorbehandelte Puh^er ergeben bei der Keimgranulierung dichtere und deshalb festere Keimgranulate, deren Festigkeit auch nach Anlagerung von nicht angranuliertem Staub bestehenbleibt. Solche Granulate sind widerstandsfähiger gegen Zerdrücken bei dem Transport z. B. in Säcken oder in begasten Kesselwagen.It has now been shown that the compressive strength of the granules can be increased, if, according to the invention, the dusty or powdery material in the pre-compressed state of the germ granulation range · The device for the production of the seed granules are compacting devices for the powder, e.g. B. elastically mounted press rolls, between which the goods on air-permeable conveyor belts guided wind, upstream. So pretreated puh ^ er result in the germ granulation denser and therefore stronger seed granules, their strength even after the accumulation of non-granulated Dust persists. Such granules are more resistant to crushing during transport z. B. in bags or in fumigated tank wagons.

In der Abbildung ist ein Vorrichtungsbeispiel zur Durchführung des Verfahrens schematisch dargestellt.An example of a device for carrying out the method is shown schematically in the figure.

Über einen Vorratsbehälter 1 mit regelbarem Auslauf läuft das zu granulierende Material, beispielsweise ein trockenes Pigment, mit etwa 0,3 °/o Feuchtigkeit einer Bandpresse 2 zu und wird hier zu plättchenartigen Gebilden verdichtet. Die Plättchen gelangen durch den Trichter 3 auf eine Schwingsiebeinrichtung 4, auf der sie wieder zerschlagen werden. Dabei entstehen einerseits unrunde Teilchen, von der Siebmaschenweite entsprechenden Teilchengröße als Keimgranulate und andererseits durch Zerschlagen und Abrieb Feinstaub. Das Gemisch aus KeimgranulatThe material to be granulated, for example, runs over a storage container 1 with a controllable outlet a dry pigment, with about 0.3% moisture to a belt press 2 and here becomes platelet-like Forms condensed. The platelets pass through the funnel 3 onto a vibrating screen device 4 on which they will be smashed again. On the one hand, this results in non-circular particles with a particle size corresponding to the screen mesh size as seed granules and on the other hand particulate matter from smashing and abrasion. The mixture of seed granules

Verfahren zum Granulieren von PulvernProcess for granulating powders

Zusatz zur Patentanmeldung F 20087 IVa/12 g
(Auslegeschrift 1 041 472)
Addition to patent application F 20087 IVa / 12 g
(Interpretation document 1 041 472)

Anmelder:Applicant:

Farbenfabriken Bayer Aktiengesellschaft,
Leverkusen-Bayerwerk
Paint factories Bayer Aktiengesellschaft,
Leverkusen-Bayerwerk

Dipl.-Ing. Julius Wehn, Leverkusen,
Dr. Richard Schlee, Leverkusen-Bayerwerk,
Dipl.-Ing. Julius Wehn, Leverkusen,
Dr. Richard Schlee, Leverkusen-Bayerwerk,

Dr. Hans Rumpf, Karlsruhe,Dr. Hans Rumpf, Karlsruhe,

Dr. Wolfgang Stroh, Leverkusen,Dr. Wolfgang Stroh, Leverkusen,

und Dipl.-Ing. Rudolf Erdmenger, Bergisch Gladbach,and Dipl.-Ing. Rudolf Erdmenger, Bergisch Gladbach,

sind als Erfinder genannt wordenhave been named as inventors

und Feinstaub wird über das Transportband 6 einem Fließbettraum 7 zugeführt, in dem, wie in der Hauptpatentanmeldung F 20087 IV a/12 g beschrieben, durch Anlagerung des Feinststaubes an die Keimgranulate unter dem Einfluß des Rolldrucks größere und festere Granulate aufgebaut werden. Die Fertiggranuläte werden über die Auslaufeinrichtung 8 abgezogen.and fine dust is fed via the conveyor belt 6 to a fluidized bed space 7 in which, as in the main patent application F 20087 IV a / 12 g, due to the accumulation of the fine dust on the germ granules larger and firmer granules are built up under the influence of the roll pressure. The finished granules are withdrawn via the outlet device 8.

Claims (5)

Patentanspruch:Claim: Verfahren zum Granulieren von Pulvern zu Granulaten gewünschter Korngröße ohne Zugabe von Bindemitteln nach Patentanmeldung F 20087 IVa/12g, bei dem das Pulver gesiebt und das ge-• siebte Gut anschließend einem an sich bekannten Rollvorgang unterworfen wird, dadurch gekennzeichnet, daß das Gut vor dem Sieb- und Rollvorgang eine Vorverdichtung erfährt.Process for granulating powders into granules of the desired grain size without adding them of binders according to patent application F 20087 IVa / 12g, in which the powder is sieved and the seventh good is then subjected to a rolling process known per se, characterized in that that the material undergoes a pre-compression before the screening and rolling process. In Betracht gezogene Druckschriften:
I.
Considered publications:
I.
Aren ds, »Die Tablettenfabrikation«, Aren ds, »The tablet production«, 5. Auflage (1950), S. 63.5th edition (1950), p. 63. Hierzu 1 Blatt Zeichnungen1 sheet of drawings
DEF21586A 1956-04-19 1956-11-06 Process for granulating powders Pending DE1051815B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEF21586A DE1051815B (en) 1956-04-19 1956-11-06 Process for granulating powders

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DEF20087A DE1041472B (en) 1956-04-19 1956-04-19 Process for granulating powders into granules of the desired grain size without the addition of binders
DEF21586A DE1051815B (en) 1956-04-19 1956-11-06 Process for granulating powders

Publications (1)

Publication Number Publication Date
DE1051815B true DE1051815B (en) 1959-03-05

Family

ID=25973967

Family Applications (1)

Application Number Title Priority Date Filing Date
DEF21586A Pending DE1051815B (en) 1956-04-19 1956-11-06 Process for granulating powders

Country Status (1)

Country Link
DE (1) DE1051815B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3167442A (en) * 1960-02-12 1965-01-26 Internat Protected Metals Inc Method of forming a resin coating on metal
DE3908022C1 (en) * 1988-09-23 1990-03-29 Degussa Ag, 6000 Frankfurt, De
CN104271254A (en) * 2012-03-30 2015-01-07 杜尔系统有限责任公司 Dry-ice cleaning device and process for a painting installation

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
None *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3167442A (en) * 1960-02-12 1965-01-26 Internat Protected Metals Inc Method of forming a resin coating on metal
DE3908022C1 (en) * 1988-09-23 1990-03-29 Degussa Ag, 6000 Frankfurt, De
CN104271254A (en) * 2012-03-30 2015-01-07 杜尔系统有限责任公司 Dry-ice cleaning device and process for a painting installation
CN104271254B (en) * 2012-03-30 2018-06-01 杜尔系统有限责任公司 For the dry ice cleaning device and method of spraying equipment
US10279453B2 (en) 2012-03-30 2019-05-07 Durr Systems Gmbh Dry-ice cleaning in a painting installation

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