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CN116098820A - Tear-type water-based lip-rounding moisturizing lip glaze capable of preventing cup from being stained and preparation method thereof - Google Patents

Tear-type water-based lip-rounding moisturizing lip glaze capable of preventing cup from being stained and preparation method thereof Download PDF

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Publication number
CN116098820A
CN116098820A CN202310174778.3A CN202310174778A CN116098820A CN 116098820 A CN116098820 A CN 116098820A CN 202310174778 A CN202310174778 A CN 202310174778A CN 116098820 A CN116098820 A CN 116098820A
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lip
parts
water
moisturizing
rounding
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CN116098820B (en
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崔晓波
宋凤蓉
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Guangdong Duoduo Biotechnology Co ltd
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Guangzhou Duoduo Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8129Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/87Polyurethanes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W90/00Enabling technologies or technologies with a potential or indirect contribution to greenhouse gas [GHG] emissions mitigation
    • Y02W90/10Bio-packaging, e.g. packing containers made from renewable resources or bio-plastics

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Abstract

本发明公开了一种撕拉式水性不沾杯丰唇保湿唇釉及其制备方法,涉及唇部护理产品技术领域。唇釉包括水、水性成膜剂、聚乙烯醇、着色剂、保湿剂、丰唇肽、抗氧剂、甜菜碱、透明质酸。本申请唇釉采用水性配方,相比于油性配方,具有更加保湿、渗透、着色的效果,且唇釉的温度稳定性和粘度可以满足储存和使用要求,采用多种保湿组分协同提高保湿效果,在唇部涂抹使用时成膜时间快,且将表面膜撕落后形成裸妆感,上色均匀且不沾杯,采用水或湿巾可以轻易卸除,无需采用卸妆水,提高使用体验感。The invention discloses a tear-off water-based non-stick cup lip plumping and moisturizing lip glaze and a preparation method thereof, and relates to the technical field of lip care products. Lip gloss includes water, water-based film former, polyvinyl alcohol, colorant, humectant, lip plumping peptide, antioxidant, betaine, hyaluronic acid. The lip glaze of this application adopts a water-based formula, which has more moisturizing, penetrating and coloring effects than the oil-based formula, and the temperature stability and viscosity of the lip glaze can meet the storage and use requirements, and a variety of moisturizing components are used to synergistically improve the moisturizing effect , when applied on the lips, the film-forming time is fast, and the surface film is torn off to form a nude makeup look, the color is even and does not stick to the cup, it can be easily removed with water or wet wipes, without using makeup remover, which improves the use experience .

Description

一种撕拉式水性不沾杯丰唇保湿唇釉及其制备方法A tear-off water-based non-stick lip plumping and moisturizing lip glaze and preparation method thereof

技术领域Technical Field

本发明涉及唇部护理产品领域,尤其涉及一种撕拉式水性不沾杯丰唇保湿唇釉及其制备方法。The invention relates to the field of lip care products, and in particular to a tear-off water-based non-stick lip plumping and moisturizing lip glaze and a preparation method thereof.

背景技术Background Art

现在市面上出现的撕拉式唇彩与普通的唇部啫喱相似,只是涂在唇部之后约5-10分钟左右会逐渐风干形成一层可以撕下来的膜,而唇彩中的颜色就印在了唇部,嘴唇上色后吃东西、喝水都不会脱色,其原理是采取直接给唇部染色的方式:使用了二甲基亚砜一类的皮肤渗透剂,利用有机物互溶的原理,可渗透到皮肤内部,与细胞膜或细胞基质中的物质结合,所以着色牢固。The peel-off lip gloss currently on the market is similar to ordinary lip gel, except that it will gradually dry to form a tearable film about 5-10 minutes after being applied to the lips, and the color of the lip gloss is printed on the lips. After the lips are colored, eating or drinking will not fade. The principle is to directly dye the lips: using skin penetrants such as dimethyl sulfoxide, using the principle of mutual solubility of organic matter, it can penetrate into the skin and combine with substances in the cell membrane or cell matrix, so the coloring is firm.

传统一般使用油脂类物质分散有机或者无机色粉或者珠光,以达到着色效果或闪亮效果,油性料体,油腻厚重,且营养成分不易添加和吸收,使用后,嘴唇干燥、紧绷感,体验不完美。Traditionally, oily substances are generally used to disperse organic or inorganic color powder or pearlescent to achieve coloring or shiny effects. Oily materials are greasy and heavy, and the nutrients are not easy to add and absorb. After use, the lips will feel dry and tight, and the experience is not perfect.

发明内容Summary of the invention

本发明提供了一种撕拉式水性不沾杯丰唇保湿唇釉及其制备方法,以提供水性不沾杯丰唇保湿唇釉,水性配方可以更亲肤更轻薄更保湿滋润,体验裸妆感,且水性体系温度稳定性好、粘度适合涂抹。The present invention provides a tear-off water-based non-stick lip plumping and moisturizing lip glaze and a preparation method thereof, so as to provide a water-based non-stick lip plumping and moisturizing lip glaze. The water-based formula can be more skin-friendly, lighter, more moisturizing and nourishing, and a nude makeup feeling can be experienced. The water-based system has good temperature stability and a viscosity suitable for coating.

为了解决上述技术问题,本发明目的之一提供了一种撕拉式水性不沾杯丰唇保湿唇釉,包括以下重量份组分:In order to solve the above technical problems, one of the purposes of the present invention is to provide a tear-off water-based non-stick lip plumping and moisturizing lip glaze, comprising the following components in parts by weight:

水:30份-60份;Water: 30-60 parts;

水性成膜剂:15份-25份;Aqueous film-forming agent: 15-25 parts;

聚乙烯醇:0.5份-2份;Polyvinyl alcohol: 0.5-2 parts;

着色剂:3份-5.5份;Colorant: 3-5.5 parts;

保湿剂:5.8份-14份;Moisturizer: 5.8-14 parts;

丰唇肽:0.2份-0.8份;Lip plumping peptide: 0.2-0.8 parts;

抗氧剂:0.1份-0.4份;Antioxidant: 0.1-0.4 parts;

甜菜碱:0.15份-0.25份;Betaine: 0.15-0.25 parts;

透明质酸:0.05份-0.12份;Hyaluronic acid: 0.05-0.12 parts;

所述水性成膜剂包括水、聚氨酯-11、聚氨酯-35、苯氧乙醇、辛甘醇。The aqueous film-forming agent includes water, polyurethane-11, polyurethane-35, phenoxyethanol and caprylyl glycol.

通过采用上述方案,本申请的撕拉式水性唇釉采用水性配方,相比于油性配方,具有更加保湿、渗透、着色的效果,同时采用多种保湿组分相互协同促进保湿性能,且唇釉的温度稳定性和粘度可以满足储存和使用要求,在唇部涂抹使用时成膜时间快,且将表面膜撕落后形成裸妆感,上色均匀且不沾杯,采用水或湿巾可以轻易卸除,无需采用卸妆水,提高使用体验感。By adopting the above scheme, the peel-off water-based lip glaze of the present application adopts a water-based formula, which has better moisturizing, penetration and coloring effects compared to oily formulas. At the same time, multiple moisturizing components are used to synergistically promote moisturizing performance, and the temperature stability and viscosity of the lip glaze can meet the storage and use requirements. When applied on the lips, the film-forming time is fast, and after the surface film is torn off, a nude makeup effect is formed. The color is even and does not stick to the cup. It can be easily removed with water or wet wipes, without the need to use makeup remover, thereby improving the use experience.

作为优选方案,还包括重量份为4份-5.5份的珠光剂,所述珠光剂包括硼硅酸铝钙、二氧化钛和氧化锡。As a preferred embodiment, the invention further comprises 4 to 5.5 parts by weight of a pearlescent agent, wherein the pearlescent agent comprises calcium aluminum borosilicate, titanium dioxide and tin oxide.

作为优选方案,所述珠光剂包括93wt%的硼硅酸铝钙、5wt%的二氧化钛和2wt%的氧化锡。As a preferred embodiment, the pearlescent agent includes 93 wt % of calcium aluminum borosilicate, 5 wt % of titanium dioxide and 2 wt % of tin oxide.

作为优选方案,所述着色剂为二氧化硅。As a preferred embodiment, the colorant is silicon dioxide.

作为优选方案,所述抗氧剂为人参(PANAX G I NSENG)提取物。As a preferred embodiment, the antioxidant is a ginseng (PANAX G I NSENG) extract.

作为优选方案,所述保湿剂包括重量份为5份-12份的二丙二醇、0.5份-1.5份的1,2-己二醇、0.3份-0.5份的对羟基苯乙酮。As a preferred embodiment, the moisturizing agent includes 5-12 parts by weight of dipropylene glycol, 0.5-1.5 parts by weight of 1,2-hexanediol, and 0.3-0.5 parts by weight of p-hydroxyacetophenone.

作为优选方案,所述水性成膜剂包括55wt%的水、13.2wt%的聚氨酯-11、30.8wt%的聚氨酯-35、0.75wt%的苯氧乙醇和0.25wt%的辛甘醇。As a preferred embodiment, the aqueous film-forming agent includes 55 wt % of water, 13.2 wt % of polyurethane-11, 30.8 wt % of polyurethane-35, 0.75 wt % of phenoxyethanol and 0.25 wt % of caprylyl glycol.

作为优选方案,包括以下重量份组分:As a preferred embodiment, the invention comprises the following components in parts by weight:

水:40份-60份;Water: 40-60 parts;

水性成膜剂:18份-23份;Aqueous film-forming agent: 18-23 parts;

聚乙烯醇:1.5份-2份;Polyvinyl alcohol: 1.5-2 parts;

着色剂:5份-6份;Colorant: 5-6 parts;

二丙二醇:8份-12份;Dipropylene glycol: 8-12 parts;

1,2-己二醇:1份-1.5份;1,2-Hexanediol: 1 part to 1.5 parts;

对羟基苯乙酮:0.4份-0.6份;p-Hydroxyacetophenone: 0.4-0.6 parts;

丰唇肽:0.1份-0.8份;Lip plumping peptide: 0.1-0.8 parts;

抗氧剂:0.1份-0.4份;Antioxidant: 0.1-0.4 parts;

甜菜碱:0.2份-0.3份;Betaine: 0.2-0.3 parts;

透明质酸:0.1份-0.12份;Hyaluronic acid: 0.1-0.12 parts;

珠光剂:5份-8份。Pearlescent agent: 5-8 parts.

为了解决上述技术问题,本发明目的之二提供了一种撕拉式水性不沾杯丰唇保湿唇釉的制备方法,包括以下步骤:In order to solve the above technical problems, the second object of the present invention is to provide a method for preparing a tear-off water-based non-stick lip plumping and moisturizing lip glaze, comprising the following steps:

(1)将水和聚乙烯醇加热到70℃-90℃高速搅拌分散均匀至透明无气泡,降至室温,获得A物料;(1) heating water and polyvinyl alcohol to 70° C.-90° C., stirring and dispersing at high speed until transparent and free of bubbles, and cooling to room temperature to obtain material A;

(2)将透明质酸、甜菜碱、丰唇肽、抗氧剂、水性成膜剂、着色剂依次加入A物料中,搅拌均匀,得到B物料;(2) adding hyaluronic acid, betaine, lip plumping peptide, antioxidant, aqueous film-forming agent, and colorant to material A in sequence, stirring evenly, to obtain material B;

(3)将珠光剂和保湿剂加入B物料中,搅拌均匀,出料即得。(3) Add pearlescent agent and moisturizing agent to material B, stir evenly, and obtain the product.

相比于现有技术,本发明实施例具有如下有益效果:Compared with the prior art, the embodiments of the present invention have the following beneficial effects:

1、本申请唇釉采用水性配方,相比于油性配方,具有更加保湿、渗透、着色的效果,且唇釉的温度稳定性和粘度可以满足储存和使用要求,在唇部涂抹使用时成膜时间快,且将表面膜撕落后形成裸妆感,上色均匀且不沾杯,采用水或湿巾可以轻易卸除,无需采用卸妆水,提高使用体验感。1. The lip glaze of this application adopts a water-based formula, which has better moisturizing, penetration and coloring effects than oily formulas. The temperature stability and viscosity of the lip glaze can meet the storage and use requirements. The film-forming time is fast when applied on the lips, and after the surface film is torn off, a nude makeup effect is formed. The color is even and does not stick to the cup. It can be easily removed with water or wet wipes, without the need to use makeup remover, thereby improving the use experience.

2、本申请采用聚乙烯醇和ST11两种水性成膜剂可以同时提高唇釉的成膜效果,减少成膜时间,粘度满足要求,同时可以保证唇釉产品的温度稳定性,方便储存。2. The present application uses two aqueous film-forming agents, polyvinyl alcohol and ST11, which can simultaneously improve the film-forming effect of the lip glaze, reduce the film-forming time, and meet the viscosity requirements. At the same time, the temperature stability of the lip glaze product can be ensured, which is convenient for storage.

3、本申请通过添加丰唇肽、甜菜碱、透明质酸等保湿组分,可以协同提高唇釉的保湿性能,同时协调保证唇釉的粘度可以满足要求,提高使用体验感。3. This application can synergistically improve the moisturizing performance of the lip glaze by adding moisturizing components such as lip plumping peptides, betaine, hyaluronic acid, etc., while coordinating to ensure that the viscosity of the lip glaze can meet the requirements and improve the user experience.

具体实施方式DETAILED DESCRIPTION

下面将结合本发明实施例,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will be combined with the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

表1-本申请实施例和对比例中原料的来源和型号Table 1 - Sources and models of raw materials in the examples and comparative examples of this application

原料名称Raw material name 型号model 厂家factory 丰唇肽Lip Peptide -- 东莞维琪科技有限公司Dongguan Vicky Technology Co., Ltd. 成膜剂Film former ST11ST11 广州福泽润Guangzhou Fuzerun 珠光剂Pearlescent Agent 19825B19825B 惠州市炜煌颜料有限公司Huizhou Weihuang Pigment Co., Ltd.

实施例1-3Examples 1-3

一种撕拉式水性不沾杯丰唇保湿唇釉,各组分含量如下表2所示,包括水、水性成膜剂、聚乙烯醇、着色剂、二丙二醇、1,2-己二醇、对羟基苯乙酮、丰唇肽、抗氧剂、甜菜碱、透明质酸、珠光剂;水性成膜剂包括水、聚氨酯-11、聚氨酯-35、苯氧乙醇、辛甘醇,在本实施例中,水性成膜剂包括55wt%的水、13.2wt%的聚氨酯-11、30.8wt%的聚氨酯-35、0.75wt%的苯氧乙醇和0.25wt%的辛甘醇,具体为ST11;着色剂为二氧化硅;珠光剂包括93wt%的硼硅酸铝钙、5wt%的二氧化钛和2wt%的氧化锡,在本实施例中,珠光剂具体为19825B;抗氧剂为人参(PANAX G I NSENG)提取物。A tear-off water-based non-stick lip plumping and moisturizing lip glaze, the contents of each component are shown in Table 2 below, including water, water-based film-forming agent, polyvinyl alcohol, colorant, dipropylene glycol, 1,2-hexanediol, p-hydroxyacetophenone, lip plumping peptide, antioxidant, betaine, hyaluronic acid, and pearlescent agent; the water-based film-forming agent includes water, polyurethane-11, polyurethane-35, phenoxyethanol, and caprylyl glycol. In this embodiment, the water-based film-forming agent includes 55wt% of water, 13.2wt% of polyurethane-11, 30.8wt% of polyurethane-35, 0.75wt% of phenoxyethanol and 0.25wt% of caprylyl glycol, specifically ST11; the colorant is silicon dioxide; the pearlescent agent includes 93wt% of calcium aluminum borosilicate, 5wt% of titanium dioxide and 2wt% of tin oxide. In this embodiment, the pearlescent agent is specifically 19825B; the antioxidant is ginseng (PANAX G I NSENG) extract.

上述一种撕拉式水性不沾杯丰唇保湿唇釉的制备方法,包括以下步骤:The preparation method of the above-mentioned tear-off water-based non-stick lip plumping and moisturizing lip glaze comprises the following steps:

(1)将水和聚乙烯醇加热高速搅拌分散均匀至透明无气泡,降至室温,获得A物料;(1) heating water and polyvinyl alcohol and stirring at high speed to disperse them uniformly until they are transparent and free of bubbles, and cooling to room temperature to obtain material A;

(2)将透明质酸、甜菜碱、丰唇肽、抗氧剂、水性成膜剂、着色剂依次加入A物料中,搅拌均匀,得到B物料;(2) adding hyaluronic acid, betaine, lip plumping peptide, antioxidant, aqueous film-forming agent, and colorant to material A in sequence, stirring evenly, to obtain material B;

(3)将珠光剂和保湿剂加入B物料中,搅拌均匀,出料即得。(3) Add pearlescent agent and moisturizing agent to material B, stir evenly, and obtain the product.

表2-本申请实施例1-3和对比例1-6中各组分及含量Table 2 - Components and contents in Examples 1-3 and Comparative Examples 1-6 of the present application

Figure BDA0004100447280000041
Figure BDA0004100447280000041

Figure BDA0004100447280000051
Figure BDA0004100447280000051

性能检测实验Performance testing experiment

1、保湿、沾杯、卸妆效果:选用平时唇部水分约在8%的志愿者,采用实施例或对比例的唇釉对志愿者唇部依次涂抹,5mi n-10mi n成膜完成后撕下唇部的一层膜,用水分测试仪测试志愿者唇部使用唇釉撕下后的水分含量数据;要求水分高于15%,结果如下表3所示。1. Moisturizing, cup-sticking and makeup removal effects: Volunteers whose lips usually have a moisture content of about 8% were selected, and the lip glazes of the embodiments or comparative examples were applied to the lips of the volunteers in sequence. After 5-10 minutes of film formation, a layer of film on the lips was torn off, and the moisture content of the lips of the volunteers after the lip glaze was torn off was tested with a moisture tester; the moisture content was required to be higher than 15%. The results are shown in Table 3 below.

2、保湿时间:对志愿者的唇部使用实施例或对比例的唇釉5mi n-10mi n成膜完成后,撕下表面的一层膜,每隔一个小时采用水分测试仪检测唇部的水分含量,当唇部的水分含量低于或等于使用前的嘴唇水分含量时,即判定为该阶段的保湿不合格,检测结果如下表3所示。2. Moisturizing time: After the lip glaze of the embodiment or the comparative example was used on the lips of volunteers for 5 min-10 min to form a film, a layer of the film on the surface was torn off, and the moisture content of the lips was tested with a moisture tester every hour. When the moisture content of the lips was lower than or equal to the moisture content of the lips before use, it was determined that the moisturizing at this stage was unqualified. The test results are shown in Table 3 below.

3、温度稳定性测试:按照唇釉标准项目感官指标GBT-27576-2011在-5℃、40℃、45℃加速测试三个月,50℃加速测试一个月,以及-5-40℃冷热交替循环一周,UV灯测试一个周,恢复常温后观测外观是否无变化,产品经离心实验3000转/分、30分钟离心实验后不分层,产品测试前后经旋转式粘度计测试粘度为30-35pa.s即合格产品,以此为判断标准,结果如表3所示。3. Temperature stability test: According to the sensory index of the lip glaze standard project GBT-27576-2011, the accelerated test was carried out at -5℃, 40℃, and 45℃ for three months, 50℃ for one month, and -5-40℃ hot and cold alternating cycle for one week, UV light test for one week, and observe whether the appearance has changed after returning to room temperature. The product did not delaminate after centrifugal test at 3000 rpm and 30 minutes. The viscosity of the product was 30-35pa.s before and after the test by a rotary viscometer, which was a qualified product. This was used as the judgment standard. The results are shown in Table 3.

4、成膜时间评估:将唇釉在测试者唇部来回涂抹三次后,观察唇釉在唇上形成保护膜所需时间,统计结果如表3所示。4. Film-forming time evaluation: After applying the lip glaze back and forth on the tester's lips three times, observe the time required for the lip glaze to form a protective film on the lips. The statistical results are shown in Table 3.

表3-本申请实施例和对比例的性能检测结果Table 3 - Performance test results of the present application examples and comparative examples

Figure BDA0004100447280000061
Figure BDA0004100447280000061

Figure BDA0004100447280000071
Figure BDA0004100447280000071

结合表3中实施例3和对比例1-2的性能检测结果可知,单纯采用聚乙烯醇作为成膜组分时,由于聚乙烯醇在体系中含量越多粘度将越大,会导致产品的涂抹轻薄度得不到要求,使用感不佳,本申请采用聚乙烯醇和ST11两种水性成膜剂可以同时提高唇釉的成膜效果,减少成膜时间,粘度满足要求,同时可以保证唇釉产品的温度稳定性,方便储存。Combining the performance test results of Example 3 and Comparative Examples 1-2 in Table 3, it can be seen that when polyvinyl alcohol is used alone as a film-forming component, the greater the content of polyvinyl alcohol in the system, the greater the viscosity will be, which will result in the product's thinness not being met and the feeling of use being poor. The present application uses two aqueous film-forming agents, polyvinyl alcohol and ST11, to simultaneously improve the film-forming effect of the lip glaze, reduce the film-forming time, meet the viscosity requirements, and at the same time ensure the temperature stability of the lip glaze product for convenient storage.

结合表3中实施例3和对比例3-6的性能检测结果可知,本申请通过添加丰唇肽、甜菜碱、透明质酸等保湿组分,可以协同提高唇釉的保湿性能,同时协调保证唇釉的粘度满足要求,提高轻薄使用体验感。Combining the performance test results of Example 3 and Comparative Examples 3-6 in Table 3, it can be seen that the present application can synergistically improve the moisturizing performance of the lip glaze by adding moisturizing components such as lip plumping peptides, betaine, hyaluronic acid, etc., while coordinating to ensure that the viscosity of the lip glaze meets the requirements, thereby improving the light and thin use experience.

以上所述的具体实施例,对本发明的目的、技术方案和有益效果进行了进一步的详细说明,应当理解,以上所述仅为本发明的具体实施例而已,并不用于限定本发明的保护范围。特别指出,对于本领域技术人员来说,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The specific embodiments described above further illustrate the purpose, technical solutions and beneficial effects of the present invention. It should be understood that the above description is only a specific embodiment of the present invention and is not intended to limit the scope of protection of the present invention. It is particularly pointed out that for those skilled in the art, any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the scope of protection of the present invention.

Claims (9)

1. The tearing type water-based lip-rounding moisturizing lip glaze is characterized by comprising the following components in parts by weight:
water: 30-60 parts;
aqueous film forming agent: 15-25 parts;
polyvinyl alcohol: 0.5-2 parts;
coloring agent: 3-6 parts;
humectant: 5.8-14 parts;
lip-rounding peptide: 0.1-0.8 parts;
an antioxidant: 0.1 to 0.4 part;
betaine: 0.15-0.25 parts;
hyaluronic acid: 0.05-0.12 parts;
the aqueous film forming agent comprises water, polyurethane-11, polyurethane-35, phenoxyethanol and octaethylene glycol.
2. The tear-type water-based non-stick cup lip rounding moisturizing lip glaze according to claim 1, further comprising 4-5.5 parts by weight of pearlizing agent, wherein the pearlizing agent comprises calcium aluminum borosilicate, titanium dioxide and tin oxide.
3. A tear-type aqueous non-stick cup, lip plumping and moisturizing lip glaze according to claim 2, wherein the pearlizing agent comprises 93wt% calcium aluminum borosilicate, 5wt% titanium dioxide and 2wt% tin oxide.
4. The tear-type aqueous non-stick cup lip rounding moisture-retaining lip glaze of claim 1, wherein the colorant is silica.
5. The tear-type water-based non-stick cup lip rounding moisturizing lip glaze according to claim 1, wherein the antioxidant is GINSENG (PANAX GINSENG) extract.
6. The tear type water-based non-stick cup lip rounding moisturizing lip glaze according to claim 1, wherein the humectant comprises 5-12 parts by weight of dipropylene glycol, 0.5-1.5 parts by weight of 1, 2-hexanediol and 0.3-0.6 parts by weight of p-hydroxyacetophenone.
7. The tear type water-based non-stick cup lip rounding moisturizing lip glaze according to claim 1, wherein the water-based film forming agent comprises 55wt% of water, 13.2wt% of polyurethane-11, 30.8wt% of polyurethane-35, 0.75wt% of phenoxyethanol and 0.25wt% of octylglycol.
8. The tear-type water-based non-stick cup lip rounding moisturizing lip glaze as claimed in claim 1, which is characterized by comprising the following components in parts by weight:
water: 40-60 parts;
aqueous film forming agent: 18-23 parts;
polyvinyl alcohol: 1.5-2 parts;
coloring agent: 5-6 parts;
dipropylene glycol: 8-12 parts;
1, 2-hexanediol: 1 to 1.5 parts;
p-hydroxyacetophenone: 0.4-0.6 parts;
lip-rounding peptide: 0.1-0.8 parts;
an antioxidant: 0.1 to 0.4 part;
betaine: 0.2-0.3 parts;
hyaluronic acid: 0.1 to 0.12 part;
pearlizing agent: 5-8 parts.
9. A method for preparing a tear-type water-based non-stick cup lip rounding moisturizing lip glaze according to any one of claims 1 to 8, which is characterized by comprising the following steps:
(1) Heating water and polyvinyl alcohol to 70-90 ℃, stirring and dispersing at high speed uniformly until the mixture is transparent and bubble-free, and cooling to room temperature to obtain a material A;
(2) Sequentially adding hyaluronic acid, betaine, lip-rounding peptide, an antioxidant, an aqueous film forming agent and a colorant into the material A, and uniformly stirring to obtain a material B;
(3) Adding pearling agent and humectant into the material B, stirring uniformly, and discharging.
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